diethyl 2,2'-(6-(2-ethoxy-2-oxoethylamino)-6-phenyl-1,4-diazepane-1,4-diyl)diacetate

Base Information

Chemical Name:diethyl 2,2'-(6-(2-ethoxy-2-oxoethylamino)-6-phenyl-1,4-diazepane-1,4-diyl)diacetate
CAS No.:1416732-11-0
Molecular Formula:C₂₃H₃₅N₃O₆
Molecular Weight:449.547
Hs Code.:

Synonyms:diethyl 2,2'-(6-(2-ethoxy-2-oxoethylamino)-6-phenyl-1,4-diazepane-1,4-diyl)diacetate

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Chemical Property of diethyl 2,2'-(6-(2-ethoxy-2-oxoethylamino)-6-phenyl-1,4-diazepane-1,4-diyl)diacetate

Chemical Property:

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Technology Process of diethyl 2,2'-(6-(2-ethoxy-2-oxoethylamino)-6-phenyl-1,4-diazepane-1,4-diyl)diacetate

There total 5 articles about diethyl 2,2'-(6-(2-ethoxy-2-oxoethylamino)-6-phenyl-1,4-diazepane-1,4-diyl)diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 1416732-10-9
diethyl 2,2'-(6-amino-6-phenyl-1,4-diazepane-1,4-diyl)diacetate

: 105-36-2
ethyl bromoacetate

: 1416732-11-0
diethyl 2,2'-(6-(2-ethoxy-2-oxoethylamino)-6-phenyl-1,4-diazepane-1,4-diyl)diacetate

Guidance literature:: With potassium carbonate; In acetonitrile; at 39.84 ℃; for 18h; Inert atmosphere;
DOI:10.1039/c2cc37544c

Reference yield:

: 1416732-07-4
1,4-bis(2,4-dimethoxybenzyl)-6-nitro-6-phenyl-1,4-diazepane

: 1416732-11-0
diethyl 2,2'-(6-(2-ethoxy-2-oxoethylamino)-6-phenyl-1,4-diazepane-1,4-diyl)diacetate

Guidance literature:: Multi-step reaction with 4 steps

1: trifluoroacetic acid / dichloromethane / 20 °C / Inert atmosphere

2: potassium carbonate / acetonitrile / 24 h / 34.84 °C / Inert atmosphere

3: hydrogen / ethanol; methanol / 3 h / 24.84 °C / Inert atmosphere

4: potassium carbonate / acetonitrile / 18 h / 39.84 °C / Inert atmosphere

With hydrogen; potassium carbonate; trifluoroacetic acid; In methanol; ethanol; dichloromethane; acetonitrile;
DOI:10.1039/c2cc37544c

Reference yield:

: 1416732-08-5
6-nitro-6-phenyl-1,4-diazepane

: 1416732-11-0
diethyl 2,2'-(6-(2-ethoxy-2-oxoethylamino)-6-phenyl-1,4-diazepane-1,4-diyl)diacetate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetonitrile / 24 h / 34.84 °C / Inert atmosphere

2: hydrogen / ethanol; methanol / 3 h / 24.84 °C / Inert atmosphere

3: potassium carbonate / acetonitrile / 18 h / 39.84 °C / Inert atmosphere

With hydrogen; potassium carbonate; In methanol; ethanol; acetonitrile;
DOI:10.1039/c2cc37544c