N-[4-Chloro-2-(2-chloro-benzoyl)-phenyl]-2-[4-(6-chloro-2-oxo-4H-benzo[d][1,3]oxazin-1-yl)-piperidin-1-yl]-acetamide hydrochloride

Base Information

Chemical Name:N-[4-Chloro-2-(2-chloro-benzoyl)-phenyl]-2-[4-(6-chloro-2-oxo-4H-benzo[d][1,3]oxazin-1-yl)-piperidin-1-yl]-acetamide hydrochloride
CAS No.:612545-17-2
Molecular Formula:C₂₈H₂₄Cl₃N₃O₄*ClH
Molecular Weight:609.336
Hs Code.:

Synonyms:N-[4-Chloro-2-(2-chloro-benzoyl)-phenyl]-2-[4-(6-chloro-2-oxo-4H-benzo[d][1,3]oxazin-1-yl)-piperidin-1-yl]-acetamide hydrochloride

Suppliers and Price of N-[4-Chloro-2-(2-chloro-benzoyl)-phenyl]-2-[4-(6-chloro-2-oxo-4H-benzo[d][1,3]oxazin-1-yl)-piperidin-1-yl]-acetamide hydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-[4-Chloro-2-(2-chloro-benzoyl)-phenyl]-2-[4-(6-chloro-2-oxo-4H-benzo[d][1,3]oxazin-1-yl)-piperidin-1-yl]-acetamide hydrochloride

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-[4-Chloro-2-(2-chloro-benzoyl)-phenyl]-2-[4-(6-chloro-2-oxo-4H-benzo[d][1,3]oxazin-1-yl)-piperidin-1-yl]-acetamide hydrochloride

There total 7 articles about N-[4-Chloro-2-(2-chloro-benzoyl)-phenyl]-2-[4-(6-chloro-2-oxo-4H-benzo[d][1,3]oxazin-1-yl)-piperidin-1-yl]-acetamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 14405-03-9
2-chloroacetamido-2’,5-dichlorobenzophenone

: 162045-31-0
1-piperidin-4-yl-1,4-dihydro-2H-3,1-benzoxazin-2-one hydrochloride

: 612545-17-2
N-[4-Chloro-2-(2-chloro-benzoyl)-phenyl]-2-[4-(6-chloro-2-oxo-4H-benzo[d][1,3]oxazin-1-yl)-piperidin-1-yl]-acetamide hydrochloride

Guidance literature:: 2-chloroacetamido-2’,5-dichlorobenzophenone; 1-piperidin-4-yl-1,4-dihydro-2H-3,1-benzoxazin-2-one hydrochloride; With potassium carbonate; In DMF (N,N-dimethyl-formamide); at 20 ℃;

With hydrogenchloride; In ethanol;

Reference yield: 61.0%

: 6-chloro-1-piperidin-4-yl-1,4-dihydrobenzo[d][1,3]oxazin-2-one hydrochloride

: 14405-03-9
2-chloroacetamido-2’,5-dichlorobenzophenone

: 612545-17-2
N-[4-Chloro-2-(2-chloro-benzoyl)-phenyl]-2-[4-(6-chloro-2-oxo-4H-benzo[d][1,3]oxazin-1-yl)-piperidin-1-yl]-acetamide hydrochloride

Guidance literature:: 6-chloro-1-piperidin-4-yl-1,4-dihydrobenzo[d][1,3]oxazin-2-one hydrochloride; 2-chloroacetamido-2’,5-dichlorobenzophenone; With potassium carbonate; In DMF (N,N-dimethyl-formamide); at 20 ℃;

With hydrogenchloride; In ethanol;

Reference yield:

: 612545-92-3
1-(tert-butyloxycarbonyl)-4-[4-chloro-(2-hydroxymethylphenylamine)]piperidine

: 612545-17-2
N-[4-Chloro-2-(2-chloro-benzoyl)-phenyl]-2-[4-(6-chloro-2-oxo-4H-benzo[d][1,3]oxazin-1-yl)-piperidin-1-yl]-acetamide hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 73 h / 0 - 20 °C

2: hydrogenchloride / diethyl ether; ethyl acetate / 4 h / 0 °C

3: potassium carbonate / DMF (N,N-dimethyl-formamide) / 20 °C

With hydrogenchloride; potassium carbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; DMF (N,N-dimethyl-formamide); diethyl ether; ethyl acetate;