Carbonic acid 1-benzyl-4-(phenyl-propionyl-amino)-piperidin-4-ylmethyl ester ethyl ester

Base Information

Chemical Name:Carbonic acid 1-benzyl-4-(phenyl-propionyl-amino)-piperidin-4-ylmethyl ester ethyl ester
CAS No.:119997-32-9
Molecular Formula:C₂₅H₃₂N₂O₄
Molecular Weight:424.54
Hs Code.:

Synonyms:Carbonic acid 1-benzyl-4-(phenyl-propionyl-amino)-piperidin-4-ylmethyl ester ethyl ester

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Chemical Property of Carbonic acid 1-benzyl-4-(phenyl-propionyl-amino)-piperidin-4-ylmethyl ester ethyl ester

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Technology Process of Carbonic acid 1-benzyl-4-(phenyl-propionyl-amino)-piperidin-4-ylmethyl ester ethyl ester

There total 9 articles about Carbonic acid 1-benzyl-4-(phenyl-propionyl-amino)-piperidin-4-ylmethyl ester ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3612-20-2
1-phenylmethyl-4-piperidone

: 119997-32-9
Carbonic acid 1-benzyl-4-(phenyl-propionyl-amino)-piperidin-4-ylmethyl ester ethyl ester

Guidance literature:: Multi-step reaction with 8 steps

2: H₂SO₄

3: conc. HCl / Heating

4: 80 percent / toluene / 240 h / Heating

5: 95 percent / LiAlH₄ / tetrahydrofuran; CH₂Cl₂ / Ambient temperature

6: 82 percent / CH₂Cl₂ / 18 h / Ambient temperature

7: 1N HCl / Ambient temperature

8: CH₂Cl₂

With hydrogenchloride; lithium aluminium tetrahydride; sulfuric acid; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/jm00125a008

Reference yield:

: 61086-04-2
4-(N-phenylamino)-1-phenylmethyl-4-piperidinylmethanol

: 119997-32-9
Carbonic acid 1-benzyl-4-(phenyl-propionyl-amino)-piperidin-4-ylmethyl ester ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / CH₂Cl₂ / 18 h / Ambient temperature

2: 1N HCl / Ambient temperature

3: CH₂Cl₂

With hydrogenchloride; In dichloromethane;
DOI:10.1021/jm00125a008

Reference yield:

: 968-86-5
1-benzyl-4-(phenylamino)piperidine-4-carbonitrile

: 119997-32-9
Carbonic acid 1-benzyl-4-(phenyl-propionyl-amino)-piperidin-4-ylmethyl ester ethyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: H₂SO₄

2: conc. HCl / Heating

3: 80 percent / toluene / 240 h / Heating

4: 95 percent / LiAlH₄ / tetrahydrofuran; CH₂Cl₂ / Ambient temperature

5: 82 percent / CH₂Cl₂ / 18 h / Ambient temperature

6: 1N HCl / Ambient temperature

7: CH₂Cl₂

With hydrogenchloride; lithium aluminium tetrahydride; sulfuric acid; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/jm00125a008