ethyl N-(4,4-dimethyl-3-oxocyclobut-1-en-1-yl)-4-(2-pyridin-3-yl-3H-imidazo[4,5-b]pyridin-3-yl)-L-phenylalaninate

Base Information

Chemical Name:ethyl N-(4,4-dimethyl-3-oxocyclobut-1-en-1-yl)-4-(2-pyridin-3-yl-3H-imidazo[4,5-b]pyridin-3-yl)-L-phenylalaninate
CAS No.:1031338-86-9
Molecular Formula:C₂₈H₂₇N₅O₃
Molecular Weight:481.554
Hs Code.:

Synonyms:ethyl N-(4,4-dimethyl-3-oxocyclobut-1-en-1-yl)-4-(2-pyridin-3-yl-3H-imidazo[4,5-b]pyridin-3-yl)-L-phenylalaninate

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Chemical Property of ethyl N-(4,4-dimethyl-3-oxocyclobut-1-en-1-yl)-4-(2-pyridin-3-yl-3H-imidazo[4,5-b]pyridin-3-yl)-L-phenylalaninate

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Technology Process of ethyl N-(4,4-dimethyl-3-oxocyclobut-1-en-1-yl)-4-(2-pyridin-3-yl-3H-imidazo[4,5-b]pyridin-3-yl)-L-phenylalaninate

There total 2 articles about ethyl N-(4,4-dimethyl-3-oxocyclobut-1-en-1-yl)-4-(2-pyridin-3-yl-3H-imidazo[4,5-b]pyridin-3-yl)-L-phenylalaninate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 59-67-6
nicotinic acid

: 1031337-90-2
ethyl 4-[(3-aminopyridin-2-yl)amino]-N-(4,4-dimethyl-3-oxocyclobut-1-en-1-yl)-L-phenylalaninate

: 1031338-86-9
ethyl N-(4,4-dimethyl-3-oxocyclobut-1-en-1-yl)-4-(2-pyridin-3-yl-3H-imidazo[4,5-b]pyridin-3-yl)-L-phenylalaninate

Guidance literature:: nicotinic acid; ethyl 4-[(3-aminopyridin-2-yl)amino]-N-(4,4-dimethyl-3-oxocyclobut-1-en-1-yl)-L-phenylalaninate; With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 18h;

With acetic acid; at 125 ℃; for 0.0833333h; Microwave irradiation;

With water; sodium hydrogencarbonate;