(1S,8S,9R,12S)-1,8-Dimethyl-12-p-tolyl-10,11,13,14,15-pentaoxa-tricyclo[7.5.1.0^2,7]pentadeca-2⁽⁷⁾,3,5-triene

Base Information

• Chemical Name: (1S,8S,9R,12S)-1,8-Dimethyl-12-p-tolyl-10,11,13,14,15-pentaoxa-tricyclo[7.5.1.0^2,7]pentadeca-2⁽⁷⁾,3,5-triene
• CAS No.: 84810-41-3
• Molecular Formula: C₁₉H₂₀O₅
• Molecular Weight: 328.365

Synonyms:(1S,8S,9R,12S)-1,8-Dimethyl-12-p-tolyl-10,11,13,14,15-pentaoxa-tricyclo[7.5.1.0^2,7]pentadeca-2⁽⁷⁾,3,5-triene

Chemical Property of (1S,8S,9R,12S)-1,8-Dimethyl-12-p-tolyl-10,11,13,14,15-pentaoxa-tricyclo[7.5.1.0^2,7]pentadeca-2⁽⁷⁾,3,5-triene

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Technology Process of (1S,8S,9R,12S)-1,8-Dimethyl-12-p-tolyl-10,11,13,14,15-pentaoxa-tricyclo[7.5.1.0^2,7]pentadeca-2⁽⁷⁾,3,5-triene

There total 3 articles about (1S,8S,9R,12S)-1,8-Dimethyl-12-p-tolyl-10,11,13,14,15-pentaoxa-tricyclo[7.5.1.0^2,7]pentadeca-2⁽⁷⁾,3,5-triene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methyl-benzaldehyde (104-87-0) + (1S,8S,9R)-1,8-Dimethyl-10,11,12-trioxa-tricyclo[7.2.1.02,7]dodeca-2(7),3,5-triene (84810-17-3) → (1S,8S,9R,12S)-1,8-Dimethyl-12-p-tolyl-10,11,13,14,15-pentaoxa-tricyclo[7.5.1.02,7]pentadeca-2(7),3,5-triene (84810-41-3)

Guidance literature:

With chlorosulfonic acid; dihydrogen peroxide; In acetic acid; for 4h; Yield given;

DOI:10.1021/ja00346a051

Reference yield:

4-methyl-benzaldehyde (104-87-0) + exo-1-methyl-3-phenylindene ozonide (84810-14-0) → (1S,8S,9R,12S)-1,8-Dimethyl-12-p-tolyl-10,11,13,14,15-pentaoxa-tricyclo[7.5.1.02,7]pentadeca-2(7),3,5-triene (84810-41-3) + (1S,8R,9R,12S)-1,8-Dimethyl-12-p-tolyl-10,11,13,14,15-pentaoxa-tricyclo[7.5.1.02,7]pentadeca-2(7),3,5-triene (84847-65-4)

Guidance literature:

With chlorosulfonic acid; dihydrogen peroxide; In acetic acid; for 2h; Yield given. Yields of byproduct given;

DOI:10.1021/ja00346a051

Reference yield:

4-methyl-benzaldehyde (104-87-0) + (1S,8R,9R)-1,8-Dimethyl-10,11,12-trioxa-tricyclo[7.2.1.02,7]dodeca-2(7),3,5-triene (84847-63-2) → (1S,8S,9R)-1,8-Dimethyl-10,11,12-trioxa-tricyclo[7.2.1.02,7]dodeca-2(7),3,5-triene (84810-17-3) + (1S,8S,9R,12S)-1,8-Dimethyl-12-p-tolyl-10,11,13,14,15-pentaoxa-tricyclo[7.5.1.02,7]pentadeca-2(7),3,5-triene (84810-41-3) + (1S,8R,9R,12S)-1,8-Dimethyl-12-p-tolyl-10,11,13,14,15-pentaoxa-tricyclo[7.5.1.02,7]pentadeca-2(7),3,5-triene (84847-65-4)

Guidance literature:

With chlorosulfonic acid; dihydrogen peroxide; In acetic acid; for 4h; Yield given. Yields of byproduct given;

DOI:10.1021/ja00346a051

upstream raw materials:

4-methyl-benzaldehyde

exo-1-methyl-3-phenylindene ozonide

(1S,8S,9R)-1,8-Dimethyl-10,11,12-trioxa-tricyclo[7.2.1.0^2,7]dodeca-2⁽⁷⁾,3,5-triene

(1S,8R,9R)-1,8-Dimethyl-10,11,12-trioxa-tricyclo[7.2.1.0^2,7]dodeca-2⁽⁷⁾,3,5-triene

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