benzyl (2,3-di((8Z,11Z)-heptadeca-8,11-dien-1-yl)-1,4-dioxaspiro[4.5]decan-8-yl)(methyl)carbamate

Base Information

Chemical Name:benzyl (2,3-di((8Z,11Z)-heptadeca-8,11-dien-1-yl)-1,4-dioxaspiro[4.5]decan-8-yl)(methyl)carbamate
CAS No.:1226892-90-5
Molecular Formula:C₅₁H₈₃NO₄
Molecular Weight:774.224
Hs Code.:

Synonyms:benzyl (2,3-di((8Z,11Z)-heptadeca-8,11-dien-1-yl)-1,4-dioxaspiro[4.5]decan-8-yl)(methyl)carbamate

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Chemical Property of benzyl (2,3-di((8Z,11Z)-heptadeca-8,11-dien-1-yl)-1,4-dioxaspiro[4.5]decan-8-yl)(methyl)carbamate

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Technology Process of benzyl (2,3-di((8Z,11Z)-heptadeca-8,11-dien-1-yl)-1,4-dioxaspiro[4.5]decan-8-yl)(methyl)carbamate

There total 6 articles about benzyl (2,3-di((8Z,11Z)-heptadeca-8,11-dien-1-yl)-1,4-dioxaspiro[4.5]decan-8-yl)(methyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 13139-17-8
N-(Benzyloxycarbonyloxy)succinimide

: 1226892-86-9
2,3-di((8Z,11Z)-heptadeca-8,11-dien-1-yl)-N-methyl-1,4-dioxaspiro[4.5]decan-8-amine

: 1226892-90-5
benzyl (2,3-di((8Z,11Z)-heptadeca-8,11-dien-1-yl)-1,4-dioxaspiro[4.5]decan-8-yl)(methyl)carbamate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/anie.201203263

Reference yield:

: 1226780-11-5
(6Z,9Z,27Z,30Z)-hexatriaconta-6,9,27,30-tetraene-18,19-diol

: 1226892-90-5
benzyl (2,3-di((8Z,11Z)-heptadeca-8,11-dien-1-yl)-1,4-dioxaspiro[4.5]decan-8-yl)(methyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / toluene / Reflux

2: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere; Reflux

3: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1002/anie.201203263

Reference yield:

: 544-35-4
ethyl (9Z,12Z)-9,12-octadecadienoate

: 1226892-90-5
benzyl (2,3-di((8Z,11Z)-heptadeca-8,11-dien-1-yl)-1,4-dioxaspiro[4.5]decan-8-yl)(methyl)carbamate

Guidance literature:: Multi-step reaction with 5 steps

1: chloro-trimethyl-silane; sodium / toluene / 3 h / 40 °C / Reflux

2: sodium tetrahydroborate / methanol; dichloromethane / 4 h / 20 °C / Inert atmosphere; Cooling with ice

3: toluene-4-sulfonic acid / toluene / Reflux

4: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere; Reflux

5: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

With sodium tetrahydroborate; lithium aluminium tetrahydride; chloro-trimethyl-silane; sodium; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1002/anie.201203263