1-{3-diphenylphosphanyl-2-[(diphenylphosphanyl)-methyl]-2-methoxymethyl-propyl}-1H-pyrazole

Base Information

Chemical Name:1-{3-diphenylphosphanyl-2-[(diphenylphosphanyl)-methyl]-2-methoxymethyl-propyl}-1H-pyrazole
CAS No.:623124-83-4
Molecular Formula:C₃₃H₃₄N₂OP₂
Molecular Weight:536.593
Hs Code.:

1-{3-diphenylphosphanyl-2-[(diphenylphosphanyl)-methyl]-2-methoxymethyl-propyl}-1<i>H</i>-pyrazole

Synonyms:1-{3-diphenylphosphanyl-2-[(diphenylphosphanyl)-methyl]-2-methoxymethyl-propyl}-1H-pyrazole

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Chemical Property of 1-{3-diphenylphosphanyl-2-[(diphenylphosphanyl)-methyl]-2-methoxymethyl-propyl}-1H-pyrazole

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Technology Process of 1-{3-diphenylphosphanyl-2-[(diphenylphosphanyl)-methyl]-2-methoxymethyl-propyl}-1H-pyrazole

There total 1 articles about 1-{3-diphenylphosphanyl-2-[(diphenylphosphanyl)-methyl]-2-methoxymethyl-propyl}-1H-pyrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 208105-72-0
2,2-bis(diphenylphosphanylmethyl)-3-(pyrazol-1-yl)propan-1-ol

: 74-88-4
methyl iodide

: 623124-83-4
1-{3-diphenylphosphanyl-2-[(diphenylphosphanyl)-methyl]-2-methoxymethyl-propyl}-1H-pyrazole

Guidance literature:: With potassium tert-butylate; potassium iodide; In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1002/ejic.200200535

Reference yield: 85.0%

: nickel(II) chloride hexahydrate

: 623124-83-4
1-{3-diphenylphosphanyl-2-[(diphenylphosphanyl)-methyl]-2-methoxymethyl-propyl}-1H-pyrazole

: 623125-01-9
[CH₂P(C₆H₅)2]2CCH₂OCH₃CH₂(C₃H₃N₂)NiCl₂

Guidance literature:: In ethanol; (Ar), ligand added to Ni salt in ethanol, stirred at 25°C for 1 h; filtered, washed (diethyl ether), dried (vac.), elem. anal.;
DOI:10.1002/ejic.200200535

Reference yield: 85.0%

: chloromethyl(1,5-cyclooctadiene)palladium(II)

: 623124-83-4
1-{3-diphenylphosphanyl-2-[(diphenylphosphanyl)-methyl]-2-methoxymethyl-propyl}-1H-pyrazole

: 623125-58-6
CH₃OCH₂CCH₂(C₃H₃N₂)[CH₂P(C₆H₅)2]2PdClCH₃

Guidance literature:: In dichloromethane; (Ar); mixed in CH2Cl2, stirred at 25°C for 10 h; evapd.(vac.), filtered, washed (petroleum ether), dried (vac.), recrystd.(CH2Cl2/Et2O), elem. anal.;
DOI:10.1002/ejic.200200535