(4-cyclopropylphenyl)-[3-((1R,2S,3S,4R,5R)-2,3,4-trisbenzyloxy-5-benzyloxymethylcyclohexyloxy)pyridin-4-yl]methanone

Base Information

Chemical Name:(4-cyclopropylphenyl)-[3-((1R,2S,3S,4R,5R)-2,3,4-trisbenzyloxy-5-benzyloxymethylcyclohexyloxy)pyridin-4-yl]methanone
CAS No.:875110-33-1
Molecular Formula:C₅₀H₄₉NO₆
Molecular Weight:759.942
Hs Code.:

Synonyms:(4-cyclopropylphenyl)-[3-((1R,2S,3S,4R,5R)-2,3,4-trisbenzyloxy-5-benzyloxymethylcyclohexyloxy)pyridin-4-yl]methanone

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Chemical Property of (4-cyclopropylphenyl)-[3-((1R,2S,3S,4R,5R)-2,3,4-trisbenzyloxy-5-benzyloxymethylcyclohexyloxy)pyridin-4-yl]methanone

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Technology Process of (4-cyclopropylphenyl)-[3-((1R,2S,3S,4R,5R)-2,3,4-trisbenzyloxy-5-benzyloxymethylcyclohexyloxy)pyridin-4-yl]methanone

There total 6 articles about (4-cyclopropylphenyl)-[3-((1R,2S,3S,4R,5R)-2,3,4-trisbenzyloxy-5-benzyloxymethylcyclohexyloxy)pyridin-4-yl]methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 776317-48-7
(4-cyclopropylphenyl)-(3-hydroxypyridin-4-yl)methanone

: 162119-25-7
(1S,2S,3S,4R,5R)-2,3,4-tris(benzyloxy)-5-[(benzyloxy)methyl]cyclohexanol

: 875110-33-1
(4-cyclopropylphenyl)-[3-((1R,2S,3S,4R,5R)-2,3,4-trisbenzyloxy-5-benzyloxymethylcyclohexyloxy)pyridin-4-yl]methanone

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In toluene; at 0 - 20 ℃; for 3h;

Reference yield:

: 130332-94-4
3-(2-(TRIMETHYLSILYL)ETHOXYMETHOXY)-PYRIDINE

: 875110-33-1
(4-cyclopropylphenyl)-[3-((1R,2S,3S,4R,5R)-2,3,4-trisbenzyloxy-5-benzyloxymethylcyclohexyloxy)pyridin-4-yl]methanone

Guidance literature:: Multi-step reaction with 5 steps

1: tert.-butyl lithium / tetrahydrofuran; pentane / 1.42 h / -78 - -70 °C

2: tetrahydrofuran; diethyl ether; pentane / 4.75 h / -78 - 20 °C

3: Dess-Martin periodane / dichloromethane / 3 h / 20 °C

4: toluene-4-sulfonic acid / tetrahydrofuran / 1 h / 65 °C

5: di-isopropyl azodicarboxylate; triphenylphosphine / toluene / 3 h / 0 - 20 °C

With di-isopropyl azodicarboxylate; tert.-butyl lithium; Dess-Martin periodane; toluene-4-sulfonic acid; triphenylphosphine; In tetrahydrofuran; diethyl ether; dichloromethane; toluene; pentane;

Reference yield:

: 776317-47-6
(4-Cyclopropylphenyl)-[3-(2-trimethyl-silylethoxymethoxy)pyridin-4-yl]methanone

: 875110-33-1
(4-cyclopropylphenyl)-[3-((1R,2S,3S,4R,5R)-2,3,4-trisbenzyloxy-5-benzyloxymethylcyclohexyloxy)pyridin-4-yl]methanone

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / tetrahydrofuran / 1 h / 65 °C

2: di-isopropyl azodicarboxylate; triphenylphosphine / toluene / 3 h / 0 - 20 °C

With di-isopropyl azodicarboxylate; toluene-4-sulfonic acid; triphenylphosphine; In tetrahydrofuran; toluene;