(1R,2S,3R,4S,5R)-2,3,4,6-tetra-O-benzyl-1-phenyl-hexane-1,2,3,4,5,6-hexaol

Base Information

Chemical Name:(1R,2S,3R,4S,5R)-2,3,4,6-tetra-O-benzyl-1-phenyl-hexane-1,2,3,4,5,6-hexaol
CAS No.:1138154-29-6
Molecular Formula:C₄₀H₄₂O₆
Molecular Weight:618.77
Hs Code.:

Synonyms:(1R,2S,3R,4S,5R)-2,3,4,6-tetra-O-benzyl-1-phenyl-hexane-1,2,3,4,5,6-hexaol

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Chemical Property of (1R,2S,3R,4S,5R)-2,3,4,6-tetra-O-benzyl-1-phenyl-hexane-1,2,3,4,5,6-hexaol

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Technology Process of (1R,2S,3R,4S,5R)-2,3,4,6-tetra-O-benzyl-1-phenyl-hexane-1,2,3,4,5,6-hexaol

There total 1 articles about (1R,2S,3R,4S,5R)-2,3,4,6-tetra-O-benzyl-1-phenyl-hexane-1,2,3,4,5,6-hexaol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6386-24-9
2,3,4,6-tetra-O-benzyl-D-galactopyranose

: 100-58-3
phenylmagnesium bromide

: 1138154-29-6
(1R,2S,3R,4S,5R)-2,3,4,6-tetra-O-benzyl-1-phenyl-hexane-1,2,3,4,5,6-hexaol

: 1138154-27-4
(1S,2S,3R,4S,5R)-2,3,4,6-tetra-O-benzyl-1-phenyl-hexane-1,2,3,4,5,6-hexaol

Guidance literature:: 2,3,4,6-tetra-O-benzyl-D-galactopyranose; phenylmagnesium bromide; With zinc dibromide; In diethyl ether; at 20 ℃; Inert atmosphere; Cooling with ice;

With water; ammonium chloride; In diethyl ether; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2009.01.014

Reference yield: 51.0%

: 1138154-29-6
(1R,2S,3R,4S,5R)-2,3,4,6-tetra-O-benzyl-1-phenyl-hexane-1,2,3,4,5,6-hexaol

: 1138154-39-8
(2,3,6-tri-O-benzyl-β-D-galactofuranosyl)benzene

: 1138154-40-1
(2,3,5,6-tetra-O-benzyl-β-D-galactofuranosyl)benzene

Guidance literature:: With 2,4-dinitrobenzenesulfonic acid; In acetonitrile; at 80 ℃; for 21h;
DOI:10.1016/j.tet.2009.01.014

Reference yield: 37.0%

: 1138154-29-6
(1R,2S,3R,4S,5R)-2,3,4,6-tetra-O-benzyl-1-phenyl-hexane-1,2,3,4,5,6-hexaol

: 1138154-39-8
(2,3,6-tri-O-benzyl-β-D-galactofuranosyl)benzene

Guidance literature:: With 2,4-dinitrobenzenesulfonic acid; In acetone; at 60 ℃; for 36h; stereospecific reaction;
DOI:10.1016/j.tet.2009.01.014