3,5-Me₂C₆H₃-N(Teoc)OTBS

Base Information

Chemical Name:3,5-Me₂C₆H₃-N(Teoc)OTBS
CAS No.:1303610-42-5
Molecular Formula:C₂₀H₃₇NO₃Si₂
Molecular Weight:395.69
Hs Code.:

3,5-Me<sub>2</sub>C<sub>6</sub>H<sub>3</sub>-N(Teoc)OTBS

Synonyms:3,5-Me₂C₆H₃-N(Teoc)OTBS

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Chemical Property of 3,5-Me₂C₆H₃-N(Teoc)OTBS

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Technology Process of 3,5-Me₂C₆H₃-N(Teoc)OTBS

There total 3 articles about 3,5-Me₂C₆H₃-N(Teoc)OTBS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 22445-41-6
3,5-dimethylphenyl iodide

: 1303610-35-6
TeocNHOTBS

: 1303610-42-5
3,5-Me₂C₆H₃-N(Teoc)OTBS

Guidance literature:: With 5-(di-tert-butylphosphino)-1′, 3′, 5′-triphenyl-1′H-[1,4′]bipyrazole; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; In toluene; at 80 ℃; for 16h; Inert atmosphere;
DOI:10.1016/j.tetlet.2010.12.034

Reference yield:

: 2916-68-9
2-(Trimethylsilyl)ethanol

: 1303610-42-5
3,5-Me₂C₆H₃-N(Teoc)OTBS

Guidance literature:: Multi-step reaction with 3 steps

1: hydroxylamine

2: triethylamine

3: 5-(di-tert-butylphosphino)-1′, 3′, 5′-triphenyl-1′H-[1,4′]bipyrazole; tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate / toluene / 16 h / 80 °C / Inert atmosphere

With 5-(di-tert-butylphosphino)-1′, 3′, 5′-triphenyl-1′H-[1,4′]bipyrazole; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; hydroxylamine; caesium carbonate; triethylamine; In toluene;
DOI:10.1016/j.tetlet.2010.12.034

Reference yield:

: 134262-94-5
N-<2-(trimethylsilyl)ethoxycarbonyl>hydroxylamine

: 1303610-42-5
3,5-Me₂C₆H₃-N(Teoc)OTBS

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine

2: 5-(di-tert-butylphosphino)-1′, 3′, 5′-triphenyl-1′H-[1,4′]bipyrazole; tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate / toluene / 16 h / 80 °C / Inert atmosphere

With 5-(di-tert-butylphosphino)-1′, 3′, 5′-triphenyl-1′H-[1,4′]bipyrazole; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; triethylamine; In toluene;
DOI:10.1016/j.tetlet.2010.12.034