[(1R,3S,4R,5R,7R)-4-Methyl-3-((E)-styryl)-2,6-dioxa-bicyclo[3.2.1]oct-7-yl]-methanol

Base Information

Chemical Name:[(1R,3S,4R,5R,7R)-4-Methyl-3-((E)-styryl)-2,6-dioxa-bicyclo[3.2.1]oct-7-yl]-methanol
CAS No.:913066-81-6
Molecular Formula:C₁₆H₂₀O₃
Molecular Weight:260.333
Hs Code.:

Synonyms:[(1R,3S,4R,5R,7R)-4-Methyl-3-((E)-styryl)-2,6-dioxa-bicyclo[3.2.1]oct-7-yl]-methanol

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Chemical Property of [(1R,3S,4R,5R,7R)-4-Methyl-3-((E)-styryl)-2,6-dioxa-bicyclo[3.2.1]oct-7-yl]-methanol

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Technology Process of [(1R,3S,4R,5R,7R)-4-Methyl-3-((E)-styryl)-2,6-dioxa-bicyclo[3.2.1]oct-7-yl]-methanol

There total 14 articles about [(1R,3S,4R,5R,7R)-4-Methyl-3-((E)-styryl)-2,6-dioxa-bicyclo[3.2.1]oct-7-yl]-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1123216-48-7
C₃₁H₄₄O₆S

: 913066-81-6
[(1R,3S,4R,5R,7R)-4-Methyl-3-((E)-styryl)-2,6-dioxa-bicyclo[3.2.1]oct-7-yl]-methanol

Guidance literature:: With potassium hexamethylsilazane; In tetrahydrofuran; toluene; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol802942j

Reference yield: 62.0%

: Toluene-4-sulfonic acid (2S,3S)-3-[(4R,5R,6S)-2-(4-methoxy-phenyl)-5-methyl-6-((E)-styryl)-[1,3]dioxan-4-ylmethyl]-oxiranylmethyl ester

: 913066-81-6
[(1R,3S,4R,5R,7R)-4-Methyl-3-((E)-styryl)-2,6-dioxa-bicyclo[3.2.1]oct-7-yl]-methanol

Guidance literature:: Toluene-4-sulfonic acid (2S,3S)-3-[(4R,5R,6S)-2-(4-methoxy-phenyl)-5-methyl-6-((E)-styryl)-[1,3]dioxan-4-ylmethyl]-oxiranylmethyl ester; With hydrogenchloride; In tetrahydrofuran; methanol; at 20 ℃; for 18h;

With sodium hydroxide; In tetrahydrofuran; methanol; at 20 ℃; for 0.0833333h;

With hydrogenchloride; In tetrahydrofuran; methanol; at 20 ℃; for 4h;
DOI:10.1021/ol061339e