N-methyl-L-leucyl-3-phenyl-D-lactyl-N-methyl-L-leucyl-D-lactyl-N-methyl-L-leucyl-3-phenyl-D-lactyl-N-methyl-L-leucyl-D-lactic acid

Base Information

Chemical Name:N-methyl-L-leucyl-3-phenyl-D-lactyl-N-methyl-L-leucyl-D-lactyl-N-methyl-L-leucyl-3-phenyl-D-lactyl-N-methyl-L-leucyl-D-lactic acid
CAS No.:153052-77-8
Molecular Formula:C₅₂H₇₈N₄O₁₃
Molecular Weight:967.21
Hs Code.:

Synonyms:N-methyl-L-leucyl-3-phenyl-D-lactyl-N-methyl-L-leucyl-D-lactyl-N-methyl-L-leucyl-3-phenyl-D-lactyl-N-methyl-L-leucyl-D-lactic acid

Suppliers and Price of N-methyl-L-leucyl-3-phenyl-D-lactyl-N-methyl-L-leucyl-D-lactyl-N-methyl-L-leucyl-3-phenyl-D-lactyl-N-methyl-L-leucyl-D-lactic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-methyl-L-leucyl-3-phenyl-D-lactyl-N-methyl-L-leucyl-D-lactyl-N-methyl-L-leucyl-3-phenyl-D-lactyl-N-methyl-L-leucyl-D-lactic acid

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of N-methyl-L-leucyl-3-phenyl-D-lactyl-N-methyl-L-leucyl-D-lactyl-N-methyl-L-leucyl-3-phenyl-D-lactyl-N-methyl-L-leucyl-D-lactic acid

There total 10 articles about N-methyl-L-leucyl-3-phenyl-D-lactyl-N-methyl-L-leucyl-D-lactyl-N-methyl-L-leucyl-3-phenyl-D-lactyl-N-methyl-L-leucyl-D-lactic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 160518-08-1
benzyl N-methyl-L-leucyl-3-phenyl-D-lactyl-N-methyl-L-leucyl-D-lactyl-N-methyl-L-leucyl-3-phenyl-D-lactyl-N-methyl-L-leucyl-D-lactate

: 153052-77-8
N-methyl-L-leucyl-3-phenyl-D-lactyl-N-methyl-L-leucyl-D-lactyl-N-methyl-L-leucyl-3-phenyl-D-lactyl-N-methyl-L-leucyl-D-lactic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 2h; under 2280 Torr;
DOI:10.7164/antibiotics.47.1322

Reference yield:

: 53363-89-6
N-t-butoxycarbonyl-N-methyl-L-leucine

: 153052-77-8
N-methyl-L-leucyl-3-phenyl-D-lactyl-N-methyl-L-leucyl-D-lactyl-N-methyl-L-leucyl-3-phenyl-D-lactyl-N-methyl-L-leucyl-D-lactic acid

Guidance literature:: Multi-step reaction with 7 steps

1: 76 percent / dicyclohexylcarbodiimide, 4-dimethylaminopyridine / CH₂Cl₂ / 1.67 h / Ambient temperature

2: 89 percent / 10percent v/v trifluoroacetic acid / CH₂Cl₂ / 0.83 h

3: 57 percent / dicyclohexylcarbodiimide, 4-dimethylaminopyridine / CH₂Cl₂ / 1.67 h / Ambient temperature

4: 90 percent / H₂ / 10percent Pd/C / ethanol / 4 h / 2280 Torr

5: 60 percent / dicyclohexylcarbodiimide, 4-dimethylaminopyridine / CH₂Cl₂ / 1.67 h / Ambient temperature

6: 93 percent / 10percent v/v trifluoroacetic acid / CH₂Cl₂ / 0.5 h

7: 96 percent / H₂ / 10percent Pd/C / ethanol / 2 h / 2280 Torr

With dmap; hydrogen; dicyclohexyl-carbodiimide; trifluoroacetic acid; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.7164/antibiotics.47.1322

Reference yield:

: 153052-70-1
benzyl N-Boc-N-methyl-L-leucyl-3-phenyl-D-lactate

: 153052-77-8
N-methyl-L-leucyl-3-phenyl-D-lactyl-N-methyl-L-leucyl-D-lactyl-N-methyl-L-leucyl-3-phenyl-D-lactyl-N-methyl-L-leucyl-D-lactic acid

Guidance literature:: Multi-step reaction with 6 steps

1: 96 percent / H₂ / 10percent Pd/C / ethanol / 7 h / 2280 Torr

2: 57 percent / dicyclohexylcarbodiimide, 4-dimethylaminopyridine / CH₂Cl₂ / 1.67 h / Ambient temperature

3: 90 percent / H₂ / 10percent Pd/C / ethanol / 4 h / 2280 Torr

4: 60 percent / dicyclohexylcarbodiimide, 4-dimethylaminopyridine / CH₂Cl₂ / 1.67 h / Ambient temperature

5: 93 percent / 10percent v/v trifluoroacetic acid / CH₂Cl₂ / 0.5 h

6: 96 percent / H₂ / 10percent Pd/C / ethanol / 2 h / 2280 Torr

With dmap; hydrogen; dicyclohexyl-carbodiimide; trifluoroacetic acid; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.7164/antibiotics.47.1322