methyl (S)-2-(2-(benzofuro[2,3-b]quinoxalin-3-yloxy)acetamido)-3-phenylpropanoate

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Chemical Name:methyl (S)-2-(2-(benzofuro[2,3-b]quinoxalin-3-yloxy)acetamido)-3-phenylpropanoate
CAS No.:1360146-60-6
Molecular Formula:C₂₆H₂₁N₃O₅
Molecular Weight:455.47
Hs Code.:

Synonyms:methyl (S)-2-(2-(benzofuro[2,3-b]quinoxalin-3-yloxy)acetamido)-3-phenylpropanoate

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Chemical Property of methyl (S)-2-(2-(benzofuro[2,3-b]quinoxalin-3-yloxy)acetamido)-3-phenylpropanoate

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Technology Process of methyl (S)-2-(2-(benzofuro[2,3-b]quinoxalin-3-yloxy)acetamido)-3-phenylpropanoate

There total 3 articles about methyl (S)-2-(2-(benzofuro[2,3-b]quinoxalin-3-yloxy)acetamido)-3-phenylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 2577-90-4
methyl (2S)-2-amino-3-phenylpropanoate

: 1360146-52-6
2-(benzofuro[3,2-b]quinoxalin-3-yloxy)acetic acid

: 1360146-60-6
methyl (S)-2-(2-(benzofuro[2,3-b]quinoxalin-3-yloxy)acetamido)-3-phenylpropanoate

Guidance literature:: With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.tetlet.2011.12.096

Reference yield:

: 68747-24-0
ethyl 2-(3-hydroxyphenoxy)acetate

: 1360146-60-6
methyl (S)-2-(2-(benzofuro[2,3-b]quinoxalin-3-yloxy)acetamido)-3-phenylpropanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: aluminum (III) chloride / 1,2-dichloro-ethane / 1 h / 80 °C / Inert atmosphere

2.1: sodium hydroxide / methanol / 0.5 h / 20 °C / Inert atmosphere

2.2: pH 1

3.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

With aluminum (III) chloride; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In methanol; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1016/j.tetlet.2011.12.096

Reference yield:

: 108-46-3
recorcinol

: 1360146-60-6
methyl (S)-2-(2-(benzofuro[2,3-b]quinoxalin-3-yloxy)acetamido)-3-phenylpropanoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / acetone / Inert atmosphere; Reflux

2.1: aluminum (III) chloride / 1,2-dichloro-ethane / 1 h / 80 °C / Inert atmosphere

3.1: sodium hydroxide / methanol / 0.5 h / 20 °C / Inert atmosphere

3.2: pH 1

4.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

With aluminum (III) chloride; potassium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In methanol; dichloromethane; 1,2-dichloro-ethane; acetone;
DOI:10.1016/j.tetlet.2011.12.096