1,10-bis(benzotriazol-1-yl)-1,10-diphenyl-2,9-decanedione bis-p-tosylhydrazone

Base Information

Chemical Name:1,10-bis(benzotriazol-1-yl)-1,10-diphenyl-2,9-decanedione bis-p-tosylhydrazone
CAS No.:189343-68-8
Molecular Formula:C₄₈H₄₈N₁₀O₄S₂
Molecular Weight:893.106
Hs Code.:

Synonyms:1,10-bis(benzotriazol-1-yl)-1,10-diphenyl-2,9-decanedione bis-p-tosylhydrazone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,10-bis(benzotriazol-1-yl)-1,10-diphenyl-2,9-decanedione bis-p-tosylhydrazone

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Technology Process of 1,10-bis(benzotriazol-1-yl)-1,10-diphenyl-2,9-decanedione bis-p-tosylhydrazone

There total 3 articles about 1,10-bis(benzotriazol-1-yl)-1,10-diphenyl-2,9-decanedione bis-p-tosylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 189343-55-3
1,10-Bis-benzotriazol-1-yl-1,10-diphenyl-decane-2,9-dione

: 189343-68-8
1,10-bis(benzotriazol-1-yl)-1,10-diphenyl-2,9-decanedione bis-p-tosylhydrazone

Guidance literature:: In benzene; for 12h; Heating;
DOI:10.1021/jo962291t

Reference yield:

: 4706-43-8
1-benzyl-1H-benzotriazole

: 189343-68-8
1,10-bis(benzotriazol-1-yl)-1,10-diphenyl-2,9-decanedione bis-p-tosylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / n-BuLi / tetrahydrofuran; hexane / 12 h / -78 - 20 °C

2: 93 percent / benzene / 12 h / Heating

With n-butyllithium; In tetrahydrofuran; hexane; benzene;
DOI:10.1021/jo962291t

Reference yield:

: 2050-23-9
diethyl suberate

: 189343-68-8
1,10-bis(benzotriazol-1-yl)-1,10-diphenyl-2,9-decanedione bis-p-tosylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / n-BuLi / tetrahydrofuran; hexane / 12 h / -78 - 20 °C

2: 93 percent / benzene / 12 h / Heating

With n-butyllithium; In tetrahydrofuran; hexane; benzene;
DOI:10.1021/jo962291t