1-(4-hydroxyphenyl)-1-thionia-5-thiacyclooctane trifluoromethanesulfonate

Base Information

Chemical Name:1-(4-hydroxyphenyl)-1-thionia-5-thiacyclooctane trifluoromethanesulfonate
CAS No.:117007-60-0
Molecular Formula:CF₃O₃S*C₁₂H₁₇OS₂
Molecular Weight:390.469
Hs Code.:

Synonyms:1-(4-hydroxyphenyl)-1-thionia-5-thiacyclooctane trifluoromethanesulfonate

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Chemical Property of 1-(4-hydroxyphenyl)-1-thionia-5-thiacyclooctane trifluoromethanesulfonate

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Technology Process of 1-(4-hydroxyphenyl)-1-thionia-5-thiacyclooctane trifluoromethanesulfonate

There total 2 articles about 1-(4-hydroxyphenyl)-1-thionia-5-thiacyclooctane trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 113504-08-8
1,5-dithioniabicyclo<3.3.0>octane bis(trifluoromethanesulphonate)

: 108-95-2,27073-41-2
phenol

: 117007-60-0
1-(4-hydroxyphenyl)-1-thionia-5-thiacyclooctane trifluoromethanesulfonate

Guidance literature:: In acetonitrile; at 0 ℃; for 3h;
DOI:10.1246/cl.1988.709 DOI:10.1016/S0040-4020(01)80348-3

Reference yield:

: 61358-15-4
1,5-dithiacyclooctane 1-oxide

: 117007-60-0
1-(4-hydroxyphenyl)-1-thionia-5-thiacyclooctane trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / CH₂Cl₂ / 3 h / -20 °C

2: 81 percent / acetonitrile / 3 h / 0 °C

In dichloromethane; acetonitrile;
DOI:10.1016/S0040-4020(01)80348-3