1-(3-methoxy-5-methylsulfonyl-4-propoxyphenyl)-4-(3,4,5-trimethoxyphenyl)-1,4-butanediol

Base Information

• Chemical Name: 1-(3-methoxy-5-methylsulfonyl-4-propoxyphenyl)-4-(3,4,5-trimethoxyphenyl)-1,4-butanediol
• CAS No.: 116681-60-8
• Molecular Formula: C₂₄H₃₄O₉S
• Molecular Weight: 498.595

Synonyms:1-(3-methoxy-5-methylsulfonyl-4-propoxyphenyl)-4-(3,4,5-trimethoxyphenyl)-1,4-butanediol

Chemical Property of 1-(3-methoxy-5-methylsulfonyl-4-propoxyphenyl)-4-(3,4,5-trimethoxyphenyl)-1,4-butanediol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(3-methoxy-5-methylsulfonyl-4-propoxyphenyl)-4-(3,4,5-trimethoxyphenyl)-1,4-butanediol

There total 15 articles about 1-(3-methoxy-5-methylsulfonyl-4-propoxyphenyl)-4-(3,4,5-trimethoxyphenyl)-1,4-butanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1-(3-methoxy-5-methylsulfonyl-4-propoxyphenyl)-4-(3,4,5-trimethoxyphenyl)-1,4-butanedione (113790-67-3) → 1-(3-methoxy-5-methylsulfonyl-4-propoxyphenyl)-4-(3,4,5-trimethoxyphenyl)-1,4-butanediol (116681-60-8)

Guidance literature:

With sodium tetrahydroborate; In ethanol; at 70 ℃; for 1h; LiAlH₄, THF, RT, 2 h;

DOI:10.1016/S0040-4039(00)82307-2

Reference yield: 100.0%

(R)-4-Hydroxy-4-(3-methanesulfonyl-5-methoxy-4-propoxy-phenyl)-1-(3,4,5-trimethoxy-phenyl)-butan-1-one (116681-65-3) → (1R,4RS)-1-(3-methoxy-5-methylsulfonyl-4-propoxyphenyl)-4-(3,4,5-trimethoxyphenyl)butane-1,4-diol (116681-60-8,121643-22-9,121643-23-0,121643-24-1,121643-25-2,121702-61-2,121702-62-3)

Guidance literature:

With sodium tetrahydroborate; In ethanol; at 70 ℃; for 0.5h;

DOI:10.1016/S0040-4039(00)82307-2

Reference yield: 100.0%

(S)-4-Hydroxy-4-(3-methanesulfonyl-5-methoxy-4-propoxy-phenyl)-1-(3,4,5-trimethoxy-phenyl)-butan-1-one (116681-64-2) → (1R,4RS)-1-(3-methoxy-5-methylsulfonyl-4-propoxyphenyl)-4-(3,4,5-trimethoxyphenyl)butane-1,4-diol (116681-60-8,121643-22-9,121643-23-0,121643-24-1,121643-25-2,121702-61-2,121702-62-3)

Guidance literature:

With sodium tetrahydroborate; In ethanol; at 70 ℃; for 0.5h;

DOI:10.1016/S0040-4039(00)82307-2

upstream raw materials:

1-(3-methoxy-5-methylsulfonyl-4-propoxyphenyl)-4-(3,4,5-trimethoxyphenyl)-1,4-butanedione

methyl (3,4,5-trimethoxyphenyl) ketone

5-iodovaniline

(R)-4-Hydroxy-4-(3-methanesulfonyl-5-methoxy-4-propoxy-phenyl)-1-(3,4,5-trimethoxy-phenyl)-butan-1-one

Downstream raw materials:

(2S,5S)-2-(3-Methanesulfonyl-5-methoxy-4-propoxy-phenyl)-5-(3,4,5-trimethoxy-phenyl)-tetrahydro-furan

(2S,5R)-2-(3-Methanesulfonyl-5-methoxy-4-propoxy-phenyl)-5-(3,4,5-trimethoxy-phenyl)-tetrahydro-furan

trans-2-(3-methoxy-5-methylsulfonyl-4-n-propoxyphenyl)-5-(3,4,5-trimethoxyphenyl)tetrahydrofuran

(-)-L 659989

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