diallyl(phenyl)phosphine oxide

Base Information

• Chemical Name: diallyl(phenyl)phosphine oxide
• CAS No.: 2501-98-6
• Molecular Formula: C₁₂H₁₅OP
• Molecular Weight: 206.224
• Mol file: 2501-98-6.mol

Synonyms:diallyl(phenyl)phosphine oxide

Chemical Property of diallyl(phenyl)phosphine oxide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of diallyl(phenyl)phosphine oxide

There total 4 articles about diallyl(phenyl)phosphine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

P,P-dichlorophenylphosphine oxide (824-72-6) + allylmagnesium bromide (1730-25-2) → diallyl(phenyl)phosphine oxide (2501-98-6)

Guidance literature:

In diethyl ether; at 20 ℃;

DOI:10.1016/S0040-4039(99)01534-8

Reference yield: 4.0%

diallyl-phenyl-phosphane (29949-75-5) → diallyl(phenyl)phosphine oxide (2501-98-6)

Guidance literature:

With dihydrogen peroxide; In tetrahydrofuran; at 0 ℃; Inert atmosphere; Schlenk technique; Glovebox;

DOI:10.1021/acs.organomet.0c00144

Reference yield:

Dichlorophenylphosphine (644-97-3) → diallyl(phenyl)phosphine oxide (2501-98-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 0 - 20 °C / Inert atmosphere; Schlenk technique; Glovebox

2: dihydrogen peroxide / tetrahydrofuran / 0 °C / Inert atmosphere; Schlenk technique; Glovebox

With dihydrogen peroxide; In tetrahydrofuran; 1: |Grignard Reaction;

DOI:10.1021/acs.organomet.0c00144

upstream raw materials:

P,P-dichlorophenylphosphine oxide

allylmagnesium bromide

Dichlorophenylphosphine

diallyl-phenyl-phosphane

Downstream raw materials:

1-phenyl-3-phospholene 1-oxide