p-tolyl 4,6-di-O-benzyl-2,3-di-O-p-methoxybenzyl-1-thio-β-Dglucopyranoside

Base Information

Chemical Name:p-tolyl 4,6-di-O-benzyl-2,3-di-O-p-methoxybenzyl-1-thio-β-Dglucopyranoside
CAS No.:1380233-74-8
Molecular Formula:C₄₃H₄₆O₇S
Molecular Weight:706.9
Hs Code.:

Synonyms:p-tolyl 4,6-di-O-benzyl-2,3-di-O-p-methoxybenzyl-1-thio-β-Dglucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-tolyl 4,6-di-O-benzyl-2,3-di-O-p-methoxybenzyl-1-thio-β-Dglucopyranoside

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Technology Process of p-tolyl 4,6-di-O-benzyl-2,3-di-O-p-methoxybenzyl-1-thio-β-Dglucopyranoside

There total 2 articles about p-tolyl 4,6-di-O-benzyl-2,3-di-O-p-methoxybenzyl-1-thio-β-Dglucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1380233-69-1
p-tolyl 2,3-di-O-(4-methoxybenzyl)-1-thio-β-D-glucopyranoside

: 100-39-0
benzyl bromide

: 1380233-74-8
p-tolyl 4,6-di-O-benzyl-2,3-di-O-p-methoxybenzyl-1-thio-β-Dglucopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at -15 - 20 ℃; for 3.5h;
DOI:10.1021/jo3002084

Reference yield:

: 219518-19-1
4-methylphenyl 4,6-O-benzylidene-1-thio-β-D-glucopyranoside

: 1380233-74-8
p-tolyl 4,6-di-O-benzyl-2,3-di-O-p-methoxybenzyl-1-thio-β-Dglucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 6.5 h / -15 - 20 °C

2: toluene-4-sulfonic acid / methanol; dichloromethane / 5 h / 20 °C

3: sodium hydride / N,N-dimethyl-formamide; mineral oil / 3.5 h / -15 - 20 °C

With sodium hydride; toluene-4-sulfonic acid; In methanol; dichloromethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/jo3002084