(S)-N-((1R,2R)-2-(dimethylamino)cyclohexylcarbamoyl)-tert-butanesulfinamide

Base Information

Chemical Name:(S)-N-((1R,2R)-2-(dimethylamino)cyclohexylcarbamoyl)-tert-butanesulfinamide
CAS No.:1001022-86-1
Molecular Formula:C₁₃H₂₇N₃O₂S
Molecular Weight:289.442
Hs Code.:

Synonyms:(S)-N-((1R,2R)-2-(dimethylamino)cyclohexylcarbamoyl)-tert-butanesulfinamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-N-((1R,2R)-2-(dimethylamino)cyclohexylcarbamoyl)-tert-butanesulfinamide

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Technology Process of (S)-N-((1R,2R)-2-(dimethylamino)cyclohexylcarbamoyl)-tert-butanesulfinamide

There total 2 articles about (S)-N-((1R,2R)-2-(dimethylamino)cyclohexylcarbamoyl)-tert-butanesulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 1046493-46-2
C₉H₁₆N₂O

: 343338-28-3
(S)-2-methylpropane-2-sulfinamide

: 1001022-86-1
(S)-N-((1R,2R)-2-(dimethylamino)cyclohexylcarbamoyl)-tert-butanesulfinamide

Guidance literature:: (S)-2-methylpropane-2-sulfinamide; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 20 ℃;

C₉H₁₆N₂O; In tetrahydrofuran; hexane; at 20 ℃; for 3h; Further stages.;
DOI:10.1021/ja075653v

Reference yield:

: 320778-92-5
(1R,2R)-N,N-dimethylcyclohexane-1,2-diamine

: 530-62-1
1,1'-carbonyldiimidazole

: 343338-28-3
(S)-2-methylpropane-2-sulfinamide

: 1001022-86-1
(S)-N-((1R,2R)-2-(dimethylamino)cyclohexylcarbamoyl)-tert-butanesulfinamide

Guidance literature:: (S)-2-methylpropane-2-sulfinamide; With potassium hydride; In tetrahydrofuran; at 0 ℃; for 0.25h; Inert atmosphere;

1,1'-carbonyldiimidazole; In tetrahydrofuran; 1,4-dioxane; at 0 - 20 ℃; Inert atmosphere;

(1R,2R)-N,N-dimethylcyclohexane-1,2-diamine; In tetrahydrofuran; 1,4-dioxane; at 20 ℃; for 20h; Inert atmosphere;
DOI:10.1016/j.tet.2012.01.048