2-(4-aminophenyl)-10-phenyl-5,10-dihydro-5λ⁶-benzo[e][1,2,4]triazolo-[1,5][1,2,4]thiadiazine-5,5-dione

Base Information

• Chemical Name: 2-(4-aminophenyl)-10-phenyl-5,10-dihydro-5λ⁶-benzo[e][1,2,4]triazolo-[1,5][1,2,4]thiadiazine-5,5-dione
• CAS No.: 1002936-95-9
• Molecular Formula: C₂₀H₁₅N₅O₂S
• Molecular Weight: 389.437

Synonyms:2-(4-aminophenyl)-10-phenyl-5,10-dihydro-5λ⁶-benzo[e][1,2,4]triazolo-[1,5][1,2,4]thiadiazine-5,5-dione

Chemical Property of 2-(4-aminophenyl)-10-phenyl-5,10-dihydro-5λ⁶-benzo[e][1,2,4]triazolo-[1,5][1,2,4]thiadiazine-5,5-dione

Chemical Property:

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Technology Process of 2-(4-aminophenyl)-10-phenyl-5,10-dihydro-5λ⁶-benzo[e][1,2,4]triazolo-[1,5][1,2,4]thiadiazine-5,5-dione

There total 1 articles about 2-(4-aminophenyl)-10-phenyl-5,10-dihydro-5λ⁶-benzo[e][1,2,4]triazolo-[1,5][1,2,4]thiadiazine-5,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

4-amino-benzoic acid (150-13-0,159246-81-8,8014-65-1) + 3-hydrazino-4-phenyl-4H-1,2,4-benzothiadiazine 1,1-dioxide (107089-81-6) → 2-(4-aminophenyl)-10-phenyl-5,10-dihydro-5λ6-benzo[e][1,2,4]triazolo-[1,5][1,2,4]thiadiazine-5,5-dione (1002936-95-9)

Guidance literature:

With trichlorophosphate; at 110 ℃;

DOI:10.1016/j.bmcl.2007.07.043

Reference yield: 70.0%

2-(4-aminophenyl)-10-phenyl-5,10-dihydro-5λ6-benzo[e][1,2,4]triazolo-[1,5][1,2,4]thiadiazine-5,5-dione (1002936-95-9) + p-toluenesulfonyl chloride (98-59-9) → C27H21N5O4S2

Guidance literature:

With pyridine; at 20 ℃; for 4h;

DOI:10.1016/j.bmcl.2007.07.043

Reference yield: 65.0%

2-(4-aminophenyl)-10-phenyl-5,10-dihydro-5λ6-benzo[e][1,2,4]triazolo-[1,5][1,2,4]thiadiazine-5,5-dione (1002936-95-9) + 2,4-Dichlorobenzenesulfonyl chloride (16271-33-3) → C26H17N5O4S2Cl2

Guidance literature:

With pyridine; at 20 ℃; for 4h;

DOI:10.1016/j.bmcl.2007.07.043

upstream raw materials:

4-amino-benzoic acid

3-hydrazino-4-phenyl-4H-1,2,4-benzothiadiazine 1,1-dioxide

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