methyl 1-(((tert-butyldiphenylsilyl)oxy)methyl)cyclohexa-2,5-dienecarboxylate

Base Information

Chemical Name:methyl 1-(((tert-butyldiphenylsilyl)oxy)methyl)cyclohexa-2,5-dienecarboxylate
CAS No.:1410840-47-9
Molecular Formula:C₂₅H₃₀O₃Si
Molecular Weight:406.597
Hs Code.:

Synonyms:methyl 1-(((tert-butyldiphenylsilyl)oxy)methyl)cyclohexa-2,5-dienecarboxylate

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Chemical Property of methyl 1-(((tert-butyldiphenylsilyl)oxy)methyl)cyclohexa-2,5-dienecarboxylate

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Technology Process of methyl 1-(((tert-butyldiphenylsilyl)oxy)methyl)cyclohexa-2,5-dienecarboxylate

There total 3 articles about methyl 1-(((tert-butyldiphenylsilyl)oxy)methyl)cyclohexa-2,5-dienecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₉H₁₂O₃

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1410840-47-9
methyl 1-(((tert-butyldiphenylsilyl)oxy)methyl)cyclohexa-2,5-dienecarboxylate

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 2h;
DOI:10.1021/ol302908a

Reference yield:

: 62627-31-0
1-(hydroxymethyl)-2,5-cyclohexadiene-1-carboxylic acid

: 1410840-47-9
methyl 1-(((tert-butyldiphenylsilyl)oxy)methyl)cyclohexa-2,5-dienecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 2 h / 0 - 20 °C

2: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 0 - 20 °C

With 1H-imidazole; thionyl chloride; In N,N-dimethyl-formamide;
DOI:10.1021/ol302908a

Reference yield:

: C₁₃H₁₈O₄

: 1410840-47-9
methyl 1-(((tert-butyldiphenylsilyl)oxy)methyl)cyclohexa-2,5-dienecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / tetrahydrofuran / 1.5 h / 0 - 20 °C

2: thionyl chloride / 2 h / 0 - 20 °C

3: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 0 - 20 °C

With 1H-imidazole; thionyl chloride; sodium hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/ol302908a