2--1,3-dithiane

Base Information

Chemical Name:2--1,3-dithiane
CAS No.:127811-86-3
Molecular Formula:C₁₆H₁₉NO₂S₂
Molecular Weight:321.464
Hs Code.:

2-<pyrrolidine-1-(benzyloxycarbonyl)-2-ylidene>-1,3-dithiane

Synonyms:2--1,3-dithiane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2--1,3-dithiane

Chemical Property:

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Technology Process of 2--1,3-dithiane

There total 6 articles about 2--1,3-dithiane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 56110-67-9
bis-(dimethylaluminium)-1,3-propenedithiolate

: 108645-62-1
N-benzyloxycarbonylproline methyl ester

: 127811-86-3
2--1,3-dithiane

: 144630-13-7
S-(3-mercaptopropyl) N-benzyloxycarbonylpyrrolidine-2-carbothioate

Guidance literature:: In dichloromethane; toluene; for 120h; Ambient temperature;

Reference yield:

: 127811-93-2
5-azidovaleric acid methyl ester

: 127811-86-3
2--1,3-dithiane

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / CH₂Cl₂; toluene / 72 h / Ambient temperature

2: 2.) pyridine / 1.) n-octane, reflux, 4 h, 2.) CH₂Cl₂, 0 deg C, 3 h

With pyridine; In dichloromethane; toluene;
DOI:10.1016/S0040-4020(01)90368-0

Reference yield:

: 2067-33-6
5-bromopentanoic acid

: 127811-86-3
2--1,3-dithiane

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) SOCl₂, 2.) NaN₃, KI / 2.) DMF

2: 75 percent / (CH₃)3Al / 48 h / 20 °C

3: octane / 3.5 h / Heating

4: pyridine

With pyridine; thionyl chloride; sodium azide; trimethylaluminum; potassium iodide; In octane;
DOI:10.1039/c39900000051