1-(4-((2-(3-chlorophenyl)-6,7-dihydro-5H-cyclopenta[b]pyridin-4-yl)amino)phenyl)-1-methylurea hydrochloride

Base Information

Chemical Name:1-(4-((2-(3-chlorophenyl)-6,7-dihydro-5H-cyclopenta[b]pyridin-4-yl)amino)phenyl)-1-methylurea hydrochloride
CAS No.:1606974-21-3
Molecular Formula:C₂₂H₂₁ClN₄O*ClH
Molecular Weight:429.349
Hs Code.:

Synonyms:1-(4-((2-(3-chlorophenyl)-6,7-dihydro-5H-cyclopenta[b]pyridin-4-yl)amino)phenyl)-1-methylurea hydrochloride

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Chemical Property of 1-(4-((2-(3-chlorophenyl)-6,7-dihydro-5H-cyclopenta[b]pyridin-4-yl)amino)phenyl)-1-methylurea hydrochloride

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Technology Process of 1-(4-((2-(3-chlorophenyl)-6,7-dihydro-5H-cyclopenta[b]pyridin-4-yl)amino)phenyl)-1-methylurea hydrochloride

There total 8 articles about 1-(4-((2-(3-chlorophenyl)-6,7-dihydro-5H-cyclopenta[b]pyridin-4-yl)amino)phenyl)-1-methylurea hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1606976-78-6
1-(4-((2-(3-chlorophenyl)-6,7-dihydro-5H-cyclopenta[b]pyridin-4-yl)amino)phenyl)-1-methylurea

: 1606974-21-3
1-(4-((2-(3-chlorophenyl)-6,7-dihydro-5H-cyclopenta[b]pyridin-4-yl)amino)phenyl)-1-methylurea hydrochloride

Guidance literature:: With hydrogenchloride; In methanol;

Reference yield:

: 1-methyl-1-(4-nitrophenyl)urea

: 1606974-21-3
1-(4-((2-(3-chlorophenyl)-6,7-dihydro-5H-cyclopenta[b]pyridin-4-yl)amino)phenyl)-1-methylurea hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: palladium 10% on activated carbon; hydrogen / methanol; ethyl acetate / 5 h / 760.05 Torr

2: hydrogenchloride / 1-methyl-pyrrolidin-2-one / 3 h / 140 °C / Microwave irradiation

3: acetic acid / tetrahydrofuran / 16 h / 20 °C

4: hydrogenchloride / methanol

With hydrogenchloride; palladium 10% on activated carbon; hydrogen; acetic acid; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; methanol; ethyl acetate;

Reference yield:

: 100-15-2
N-methyl(p-nitroaniline)

: 1606974-21-3
1-(4-((2-(3-chlorophenyl)-6,7-dihydro-5H-cyclopenta[b]pyridin-4-yl)amino)phenyl)-1-methylurea hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: acetic acid / tetrahydrofuran / 24 h / 20 °C

2: palladium 10% on activated carbon; hydrogen / methanol; ethyl acetate / 5 h / 760.05 Torr

3: hydrogenchloride / 1-methyl-pyrrolidin-2-one / 3 h / 140 °C / Microwave irradiation

4: acetic acid / tetrahydrofuran / 16 h / 20 °C

5: hydrogenchloride / methanol

With hydrogenchloride; palladium 10% on activated carbon; hydrogen; acetic acid; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; methanol; ethyl acetate;