1-(4-((2-(3-chlorophenyl)-6,7-dihydro-5H-cyclopenta[b]pyridin-4-yl)amino)phenyl)-1-methylurea

Base Information

Chemical Name:1-(4-((2-(3-chlorophenyl)-6,7-dihydro-5H-cyclopenta[b]pyridin-4-yl)amino)phenyl)-1-methylurea
CAS No.:1606976-78-6
Molecular Formula:C₂₂H₂₁ClN₄O
Molecular Weight:392.888
Hs Code.:

Synonyms:1-(4-((2-(3-chlorophenyl)-6,7-dihydro-5H-cyclopenta[b]pyridin-4-yl)amino)phenyl)-1-methylurea

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Chemical Property of 1-(4-((2-(3-chlorophenyl)-6,7-dihydro-5H-cyclopenta[b]pyridin-4-yl)amino)phenyl)-1-methylurea

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Technology Process of 1-(4-((2-(3-chlorophenyl)-6,7-dihydro-5H-cyclopenta[b]pyridin-4-yl)amino)phenyl)-1-methylurea

There total 7 articles about 1-(4-((2-(3-chlorophenyl)-6,7-dihydro-5H-cyclopenta[b]pyridin-4-yl)amino)phenyl)-1-methylurea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1606976-77-5
N₁-(2-(3-chlorophenyl)-6,7-dihydro-5H-cyclopenta[b]pyridin-4-yl)-N₄-methylbenzene-1,4-diamine

: 917-61-3
sodium isocyanate

: 1606976-78-6
1-(4-((2-(3-chlorophenyl)-6,7-dihydro-5H-cyclopenta[b]pyridin-4-yl)amino)phenyl)-1-methylurea

Guidance literature:: With acetic acid; In tetrahydrofuran; at 20 ℃; for 16h;

Reference yield:

: 100-15-2
N-methyl(p-nitroaniline)

: 1606976-78-6
1-(4-((2-(3-chlorophenyl)-6,7-dihydro-5H-cyclopenta[b]pyridin-4-yl)amino)phenyl)-1-methylurea

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid / tetrahydrofuran / 24 h / 20 °C

2: palladium 10% on activated carbon; hydrogen / methanol; ethyl acetate / 5 h / 760.05 Torr

3: hydrogenchloride / 1-methyl-pyrrolidin-2-one / 3 h / 140 °C / Microwave irradiation

4: acetic acid / tetrahydrofuran / 16 h / 20 °C

With hydrogenchloride; palladium 10% on activated carbon; hydrogen; acetic acid; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; methanol; ethyl acetate;

Reference yield:

: 1040323-21-4
1-(4-aminophenyl)-1-methylurea

: 1606976-78-6
1-(4-((2-(3-chlorophenyl)-6,7-dihydro-5H-cyclopenta[b]pyridin-4-yl)amino)phenyl)-1-methylurea

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / 1-methyl-pyrrolidin-2-one / 3 h / 140 °C / Microwave irradiation

2: acetic acid / tetrahydrofuran / 16 h / 20 °C

With hydrogenchloride; acetic acid; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one;