prop-2-yn-1-yl 3,4,6-tri-O-benzyl-2-O-[2,3,4,6-tetra-O-benzyl α-D-mannopyranosyl] α-Dmannopyranoside

Base Information

Chemical Name:prop-2-yn-1-yl 3,4,6-tri-O-benzyl-2-O-[2,3,4,6-tetra-O-benzyl α-D-mannopyranosyl] α-Dmannopyranoside
CAS No.:1384752-85-5
Molecular Formula:C₆₄H₆₆O₁₁
Molecular Weight:1011.22
Hs Code.:

Synonyms:prop-2-yn-1-yl 3,4,6-tri-O-benzyl-2-O-[2,3,4,6-tetra-O-benzyl α-D-mannopyranosyl] α-Dmannopyranoside

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Chemical Property of prop-2-yn-1-yl 3,4,6-tri-O-benzyl-2-O-[2,3,4,6-tetra-O-benzyl α-D-mannopyranosyl] α-Dmannopyranoside

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Technology Process of prop-2-yn-1-yl 3,4,6-tri-O-benzyl-2-O-[2,3,4,6-tetra-O-benzyl α-D-mannopyranosyl] α-Dmannopyranoside

There total 3 articles about prop-2-yn-1-yl 3,4,6-tri-O-benzyl-2-O-[2,3,4,6-tetra-O-benzyl α-D-mannopyranosyl] α-Dmannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1384752-81-1
C₃₀H₃₂O₆

: 1384752-77-5
1-ethynylcyclohexyl 2,3,4,6-tetra-O-benzyl α-D-mannopyranoside

: 1384752-85-5
prop-2-yn-1-yl 3,4,6-tri-O-benzyl-2-O-[2,3,4,6-tetra-O-benzyl α-D-mannopyranosyl] α-Dmannopyranoside

Guidance literature:: With gold(III) chloride; silver hexafluoroantimonate; In dichloromethane; acetonitrile; at 20 ℃; for 8h; Inert atmosphere;
DOI:10.1039/c2cc32649c

Reference yield:

: C₁₄H₂₂O₆

: 1384752-85-5
prop-2-yn-1-yl 3,4,6-tri-O-benzyl-2-O-[2,3,4,6-tetra-O-benzyl α-D-mannopyranosyl] α-Dmannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / N,N-dimethyl-formamide / Inert atmosphere

2: silver hexafluoroantimonate; gold(III) chloride / dichloromethane; acetonitrile / 8 h / 20 °C / Inert atmosphere

With gold(III) chloride; silver hexafluoroantimonate; sodium hydride; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c2cc32649c

Reference yield:

: 100-39-0
benzyl bromide

: 1384752-85-5
prop-2-yn-1-yl 3,4,6-tri-O-benzyl-2-O-[2,3,4,6-tetra-O-benzyl α-D-mannopyranosyl] α-Dmannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / N,N-dimethyl-formamide / Inert atmosphere

2: silver hexafluoroantimonate; gold(III) chloride / dichloromethane; acetonitrile / 8 h / 20 °C / Inert atmosphere

With gold(III) chloride; silver hexafluoroantimonate; sodium hydride; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c2cc32649c