ethoxycarbonyl-α-(4-methylsulfonylphenyl)methyl 4-benzyloxyphenylacetate

Base Information

Chemical Name:ethoxycarbonyl-α-(4-methylsulfonylphenyl)methyl 4-benzyloxyphenylacetate
CAS No.:862252-78-6
Molecular Formula:C₂₆H₂₆O₇S
Molecular Weight:482.554
Hs Code.:

Synonyms:ethoxycarbonyl-α-(4-methylsulfonylphenyl)methyl 4-benzyloxyphenylacetate

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Chemical Property of ethoxycarbonyl-α-(4-methylsulfonylphenyl)methyl 4-benzyloxyphenylacetate

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Technology Process of ethoxycarbonyl-α-(4-methylsulfonylphenyl)methyl 4-benzyloxyphenylacetate

There total 3 articles about ethoxycarbonyl-α-(4-methylsulfonylphenyl)methyl 4-benzyloxyphenylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: ethyl α-bromo-(4-methylsulfonylphenyl)acetate

: 6547-53-1
2-[4-(benzyloxy)benzyl]acetic acid

: 862252-78-6
ethoxycarbonyl-α-(4-methylsulfonylphenyl)methyl 4-benzyloxyphenylacetate

Guidance literature:: With triethylamine; In tetrahydrofuran; Heating;
DOI:10.1016/j.bmc.2005.04.055

Reference yield:

: 156-38-7
4-hydroxyphenylacetate

: 862252-78-6
ethoxycarbonyl-α-(4-methylsulfonylphenyl)methyl 4-benzyloxyphenylacetate

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃; KI / dimethylformamide / Heating

2: 88 percent / triethylamine / tetrahydrofuran / Heating

With potassium carbonate; triethylamine; potassium iodide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2005.04.055

Reference yield:

: 100-44-7
benzyl chloride

: 862252-78-6
ethoxycarbonyl-α-(4-methylsulfonylphenyl)methyl 4-benzyloxyphenylacetate

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃; KI / dimethylformamide / Heating

2: 88 percent / triethylamine / tetrahydrofuran / Heating

With potassium carbonate; triethylamine; potassium iodide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2005.04.055