2-bromo-4-[4-(3,5-dichlorophenyl)-4-trifluoromethyl-4,5-dihydro-3H-pyrrol-2-yl]benzylamine

Base Information

Chemical Name:2-bromo-4-[4-(3,5-dichlorophenyl)-4-trifluoromethyl-4,5-dihydro-3H-pyrrol-2-yl]benzylamine
CAS No.:1159792-41-2
Molecular Formula:C₁₈H₁₄BrCl₂F₃N₂
Molecular Weight:466.128
Hs Code.:

Synonyms:2-bromo-4-[4-(3,5-dichlorophenyl)-4-trifluoromethyl-4,5-dihydro-3H-pyrrol-2-yl]benzylamine

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Chemical Property of 2-bromo-4-[4-(3,5-dichlorophenyl)-4-trifluoromethyl-4,5-dihydro-3H-pyrrol-2-yl]benzylamine

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Technology Process of 2-bromo-4-[4-(3,5-dichlorophenyl)-4-trifluoromethyl-4,5-dihydro-3H-pyrrol-2-yl]benzylamine

There total 12 articles about 2-bromo-4-[4-(3,5-dichlorophenyl)-4-trifluoromethyl-4,5-dihydro-3H-pyrrol-2-yl]benzylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1174731-71-5
methanesulfonic acid 2-bromo-4-[4-(3,5-dichlorophenyl)-4-trifluoromethyl-4,5-dihydro-3H-pyrrol-2-yl]benzyl ester

: 1159792-41-2
2-bromo-4-[4-(3,5-dichlorophenyl)-4-trifluoromethyl-4,5-dihydro-3H-pyrrol-2-yl]benzylamine

Guidance literature:: With ammonia; In tetrahydrofuran; methanol; water; at 20 ℃; for 20h;

Reference yield:

: 1159792-40-1
N-[2-bromo-4-[4-(3,5-dichlorophenyl)-4-trifluoromethyl-4,5-dihydro-3H-pyrrole-2-yl] phenylmethyl] phthalimide

: 1159792-41-2
2-bromo-4-[4-(3,5-dichlorophenyl)-4-trifluoromethyl-4,5-dihydro-3H-pyrrol-2-yl]benzylamine

Guidance literature:: With hydrazine hydrate; In ethanol; for 2h; Reflux;

Reference yield:

: 1174731-66-8
acetic acid 2-bromo-4-(trimethylsilanylmethyl-carbamoyl)-benzylester

: 1159792-41-2
2-bromo-4-[4-(3,5-dichlorophenyl)-4-trifluoromethyl-4,5-dihydro-3H-pyrrol-2-yl]benzylamine

Guidance literature:: Multi-step reaction with 6 steps

1: Lawessons reagent / tetrahydrofuran / 3 h / Reflux

2: potassium carbonate / N,N-dimethyl-formamide / 4 h / 0 °C

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 8 h / 0 - 20 °C / Inert atmosphere

4: sodium methylate; methanol / 1 h / 20 °C

5: triethylamine / tetrahydrofuran / 1 h / 20 °C

6: methanol; ammonium hydroxide / tetrahydrofuran / 12 h / 20 °C

With Lawessons reagent; methanol; ammonium hydroxide; tetrabutyl ammonium fluoride; sodium methylate; potassium carbonate; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;