2-[benzyloxy-(3-[1,3]dioxolan-2-ylpyridin-2-yl)methyl]-1-methyl-1H-indole

Base Information

• Chemical Name: 2-[benzyloxy-(3-[1,3]dioxolan-2-ylpyridin-2-yl)methyl]-1-methyl-1H-indole
• CAS No.: 1220891-97-3
• Molecular Formula: C₂₅H₂₄N₂O₃
• Molecular Weight: 400.477

Synonyms:2-[benzyloxy-(3-[1,3]dioxolan-2-ylpyridin-2-yl)methyl]-1-methyl-1H-indole

Chemical Property of 2-[benzyloxy-(3-[1,3]dioxolan-2-ylpyridin-2-yl)methyl]-1-methyl-1H-indole

Chemical Property:

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Technology Process of 2-[benzyloxy-(3-[1,3]dioxolan-2-ylpyridin-2-yl)methyl]-1-methyl-1H-indole

There total 1 articles about 2-[benzyloxy-(3-[1,3]dioxolan-2-ylpyridin-2-yl)methyl]-1-methyl-1H-indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

[3-(1,3-dioxolan-2-yl)pyridin-2-yl](1-methyl-1H-indol-2-yl)methanol (1220891-96-2) + benzyl bromide (100-39-0) → 2-[benzyloxy-(3-[1,3]dioxolan-2-ylpyridin-2-yl)methyl]-1-methyl-1H-indole (1220891-97-3)

Guidance literature:

[3-(1,3-dioxolan-2-yl)pyridin-2-yl](1-methyl-1H-indol-2-yl)methanol; With sodium hydride; potassium iodide; In tetrahydrofuran; mineral oil; at 20 ℃; for 0.5h;

benzyl bromide; In tetrahydrofuran; mineral oil; at 20 ℃; for 18h;

DOI:10.1002/chem.200901947

Reference yield: 34.0%

2-[benzyloxy-(3-[1,3]dioxolan-2-ylpyridin-2-yl)methyl]-1-methyl-1H-indole (1220891-97-3) → 11-benzyloxy-10-methyl-10H-pyrido[2,3-b]carbazole (1220891-98-4)

Guidance literature:

With hydrogenchloride; In water; acetone; at 20 ℃; for 72h;

DOI:10.1002/chem.200901947

upstream raw materials:

[3-(1,3-dioxolan-2-yl)pyridin-2-yl](1-methyl-1H-indol-2-yl)methanol

benzyl bromide

Downstream raw materials:

11-benzyloxy-10-methyl-10H-pyrido[2,3-b]carbazole

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