2-(4-Hydrazinylphenyl)-N-methylethanesulfonamide hydrochloride

Base Information

• Chemical Name: 2-(4-Hydrazinylphenyl)-N-methylethanesulfonamide hydrochloride
• CAS No.: 42381-27-1
• Molecular Formula: C9H15N3O2S^.HCl
• Molecular Weight: 265.764
• Hs Code.: 2935009090
• European Community (EC) Number: 610-023-3
• DSSTox Substance ID: DTXSID40602087
• Mol file: 42381-27-1.mol

Synonyms:42381-27-1;2-(4-Hydrazinylphenyl)-N-methylethanesulfonamide hydrochloride;4-Hydrazino-N-methylbenzeneethanesulfonamide hydrochloride;2-(4-hydrazinylphenyl)-N-methylethanesulfonamide;hydrochloride;4-hydrazino-n-methyl benzene ethane sulfonamide hydrochloride;C9H16ClN3O2S;p-[beta-(Methylsulfonamido)ethyl]phenylhydrazine hydrochloride;SCHEMBL2869306;DTXSID40602087;2-(4-Hydrazinylphenyl)-N-methylethanesulfonamidehydrochloride;4-Hydrazino-N-metyl benzene ethane sulfonamide hydrochloride;AKOS015999778;SB81698;2-(4-Hydrazinylphenyl)-N-methylethane-1-sulfonamide--hydrogen chloride (1/1)

Chemical Property of 2-(4-Hydrazinylphenyl)-N-methylethanesulfonamide hydrochloride

Chemical Property:

• Appearance/Colour: yellow to light yellow crystal powder
• Vapor Pressure: 7.79E-09mmHg at 25°C
• Boiling Point: 459.2 °C at 760 mmHg
• Flash Point: 231.5 °C
• PSA: 92.60000
• LogP: 3.11090
• Hydrogen Bond Donor Count: 4
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 5
• Exact Mass: 265.0651756
• Heavy Atom Count: 16
• Complexity: 266

Purity/Quality:

99% ^*data from raw suppliers

4-Hydrazinyl-N-methylbenzeneethanesulfonamide hydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CNS(=O)(=O)CCC1=CC=C(C=C1)NN.Cl
• Uses: An intermediate in the preparation of antimigraine drug Naratriptan (N378730). Naratriptan intermediate

Technology Process of 2-(4-Hydrazinylphenyl)-N-methylethanesulfonamide hydrochloride

There total 3 articles about 2-(4-Hydrazinylphenyl)-N-methylethanesulfonamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2-(4-amino-phenyl)ethanesulfonic acid methylamide (98623-16-6) → 2-(4-hydrazinylphenyl)-N-methylethane-1-sulfonamide hydrochloride (42381-27-1)

Guidance literature:

2-(4-amino-phenyl)ethanesulfonic acid methylamide; With sodium nitrite;

With hydrogenchloride; tin(ll) chloride;

Reference yield: 67.0%

→ 4-[2-(3-Cyanopropylidene)hydrazino]-N-methyl-benzeneethanesulphonamide + 2-(4-hydrazinylphenyl)-N-methylethane-1-sulfonamide hydrochloride (42381-27-1)

Guidance literature:

Reference yield: 66.0%

→ 2-(4-hydrazinylphenyl)-N-methylethane-1-sulfonamide hydrochloride (42381-27-1)

Guidance literature:

upstream raw materials:

2-(4-amino-phenyl)ethanesulfonic acid methylamide

Downstream raw materials:

C₁₇H₁₉N₃O₂S₂

C₁₉H₁₈F₃N₃O₂S

C₂₀H₂₀F₃N₃O₂S

2-(3-phenylsulfanyl-1H-indol-5-yl)ethanesulfonicacid methylamide

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