2-methoxyethyl 2-(4-{4-[(2',3'-O-isopropylideneuridin-5'-yloxy)diphenylmethyl]-1H-1,2,3-triazol-1-yl}butoxy)benzoate

Base Information

Chemical Name:2-methoxyethyl 2-(4-{4-[(2',3'-O-isopropylideneuridin-5'-yloxy)diphenylmethyl]-1H-1,2,3-triazol-1-yl}butoxy)benzoate
CAS No.:1299596-19-2
Molecular Formula:C₄₁H₄₅N₅O₁₀
Molecular Weight:767.836
Hs Code.:

Synonyms:2-methoxyethyl 2-(4-{4-[(2',3'-O-isopropylideneuridin-5'-yloxy)diphenylmethyl]-1H-1,2,3-triazol-1-yl}butoxy)benzoate

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Chemical Property of 2-methoxyethyl 2-(4-{4-[(2',3'-O-isopropylideneuridin-5'-yloxy)diphenylmethyl]-1H-1,2,3-triazol-1-yl}butoxy)benzoate

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Technology Process of 2-methoxyethyl 2-(4-{4-[(2',3'-O-isopropylideneuridin-5'-yloxy)diphenylmethyl]-1H-1,2,3-triazol-1-yl}butoxy)benzoate

There total 3 articles about 2-methoxyethyl 2-(4-{4-[(2',3'-O-isopropylideneuridin-5'-yloxy)diphenylmethyl]-1H-1,2,3-triazol-1-yl}butoxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1263214-78-3
2-{4-[4-(hydroxy-diphenyl-methyl)-[1,2,3]triazol-1-yl]-butoxy}-benzoic acid 2-methoxy-ethyl ester

: 362-43-6
2',3'-O-isopropylideneuridine

: 1299596-19-2
2-methoxyethyl 2-(4-{4-[(2',3'-O-isopropylideneuridin-5'-yloxy)diphenylmethyl]-1H-1,2,3-triazol-1-yl}butoxy)benzoate

Guidance literature:: With Tris(pentafluorophenyl)methane; In dichloromethane; Reflux;
DOI:10.1002/ejoc.201001677

Reference yield:

: 119-61-9
benzophenone

: 1299596-19-2
2-methoxyethyl 2-(4-{4-[(2',3'-O-isopropylideneuridin-5'-yloxy)diphenylmethyl]-1H-1,2,3-triazol-1-yl}butoxy)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -10 °C / Inert atmosphere

1.2: 3 h / -10 °C / Inert atmosphere

1.3: 0 - 20 °C / Inert atmosphere

2.1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / tetrahydrofuran; water / 25 °C / Inert atmosphere

3.1: Tris(pentafluorophenyl)methane / dichloromethane / Reflux

With n-butyllithium; copper(ll) sulfate pentahydrate; Tris(pentafluorophenyl)methane; sodium L-ascorbate; In tetrahydrofuran; hexane; dichloromethane; water;
DOI:10.1002/ejoc.201001677

Reference yield:

: 3923-52-2
1,1-diphenyl-2-propyn-1-ol

: 1299596-19-2
2-methoxyethyl 2-(4-{4-[(2',3'-O-isopropylideneuridin-5'-yloxy)diphenylmethyl]-1H-1,2,3-triazol-1-yl}butoxy)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / tetrahydrofuran; water / 25 °C / Inert atmosphere

2: Tris(pentafluorophenyl)methane / dichloromethane / Reflux

With copper(ll) sulfate pentahydrate; Tris(pentafluorophenyl)methane; sodium L-ascorbate; In tetrahydrofuran; dichloromethane; water;
DOI:10.1002/ejoc.201001677