2-[4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]phenyl]-6-[[(trifluoromethyl)sulfonyl]oxy]benzo[b]thiophen-3-yl 4-[2-(1-piperidinyl)ethoxy]phenyl ketone

Base Information

Chemical Name:2-[4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]phenyl]-6-[[(trifluoromethyl)sulfonyl]oxy]benzo[b]thiophen-3-yl 4-[2-(1-piperidinyl)ethoxy]phenyl ketone
CAS No.:185416-86-8
Molecular Formula:C₃₅H₄₀F₃NO₆S₂Si
Molecular Weight:719.918
Hs Code.:

2-[4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]phenyl]-6-[[(trifluoromethyl)sulfonyl]oxy]benzo[b]thiophen-3-yl 4-[2-(1-piperidinyl)ethoxy]phenyl ketone

Synonyms:2-[4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]phenyl]-6-[[(trifluoromethyl)sulfonyl]oxy]benzo[b]thiophen-3-yl 4-[2-(1-piperidinyl)ethoxy]phenyl ketone

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Chemical Property of 2-[4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]phenyl]-6-[[(trifluoromethyl)sulfonyl]oxy]benzo[b]thiophen-3-yl 4-[2-(1-piperidinyl)ethoxy]phenyl ketone

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Technology Process of 2-[4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]phenyl]-6-[[(trifluoromethyl)sulfonyl]oxy]benzo[b]thiophen-3-yl 4-[2-(1-piperidinyl)ethoxy]phenyl ketone

There total 2 articles about 2-[4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]phenyl]-6-[[(trifluoromethyl)sulfonyl]oxy]benzo[b]thiophen-3-yl 4-[2-(1-piperidinyl)ethoxy]phenyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 37595-74-7
N,N-phenylbistrifluoromethane-sulfonimide

: 174264-46-1
2-[4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]phenyl]-6-hydroxybenzo[b]thiophen-3-yl 4-[2-(1-piperidinyl)ethoxy]phenyl ketone

: 185416-86-8
2-[4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]phenyl]-6-[[(trifluoromethyl)sulfonyl]oxy]benzo[b]thiophen-3-yl 4-[2-(1-piperidinyl)ethoxy]phenyl ketone

Guidance literature:: With triethylamine; In 1,2-dichloro-ethane; Ambient temperature;
DOI:10.1021/jm9606352

Reference yield:

: 185416-86-8
2-[4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]phenyl]-6-[[(trifluoromethyl)sulfonyl]oxy]benzo[b]thiophen-3-yl 4-[2-(1-piperidinyl)ethoxy]phenyl ketone

Guidance literature:

Reference yield:

: 6737-42-4
1,3-bis-(diphenylphosphino)propane

: 185416-86-8
2-[4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]phenyl]-6-[[(trifluoromethyl)sulfonyl]oxy]benzo[b]thiophen-3-yl 4-[2-(1-piperidinyl)ethoxy]phenyl ketone

: 189940-52-1
2-(4-hydroxyphenyl)-3-[4-[2-(1-piperidinyl)ethoxy]benzoyl]benzo[b]thiophene-6-carboxylic acid methyl ester

Guidance literature:: With hydrogenchloride; ammonium hydroxide; triethylamine; palladium diacetate; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;