Isobornyl 2-methyl-2-propenoate

Base Information

• Chemical Name: Isobornyl 2-methyl-2-propenoate
• CAS No.: 28854-39-9
• Molecular Formula: C₁₄H₂₂O₂
• Molecular Weight: 222.327
• Hs Code.: 2916140000
• Mol file: 28854-39-9.mol

Synonyms:Isobornyl Methacrylate;[(1R,4R,6R)-1,7,7-Trimethyl-6-bicyclo[2.2.1]heptanyl] 2-methylprop-2-enoate;

Chemical Property of Isobornyl 2-methyl-2-propenoate

Chemical Property:

• Boiling Point: 160.5 °C at 760 mmHg
• Flash Point: 74.2 °C
• PSA: 26.30000
• LogP: 3.32050

Purity/Quality:

98%Min ^*data from raw suppliers

ISOBORNYL 2-METHYL-2-PROPENOATE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Isobornyl 2-methyl-2-propenoate

There total 12 articles about Isobornyl 2-methyl-2-propenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.7%

tempol (2226-96-2) + 4-methoxy-phenol (150-76-5) + methacrylic acid methyl ester (80-62-6,114512-63-9,143476-91-9,25188-98-1,9011-14-7) + iso-Bornyl acetate (71424-71-0) → isobornyl methacrylate (16868-12-5,28854-39-9,93120-52-6)

Guidance literature:

With LiOH; calcium oxide; In methanol;

Reference yield: 93.0%

borneol (464-43-7,464-45-9,507-70-0,6627-72-1,10334-13-1,10385-78-1,24393-70-2,124-76-5,16725-71-6) + methacrylic acid methyl ester (80-62-6,114512-63-9,143476-91-9,25188-98-1,9011-14-7) → (1S,2S,4S)-1,7,7-trimethylbicyclo[2.2.1]heptan-2-yl methacrylate (28854-39-9,93120-52-6)

Guidance literature:

With tetramethylammonium methyl carbonate; at 70 ℃; for 16h; Molecular sieve; Green chemistry;

DOI:10.1039/c7gc03858e

Reference yield: 92.0%

poly(methacrylic acid) (79-41-4,25087-26-7,50867-57-7) + camphene (5794-04-7) → (1S,2S,4S)-1,7,7-trimethylbicyclo[2.2.1]heptan-2-yl methacrylate (28854-39-9,93120-52-6)

Guidance literature:

With bisdodecylphenyliodonium hexafluoroantimonate; hydroquinone; for 0.333333h; Reagent/catalyst; UV-irradiation;

upstream raw materials:

methacryloyl anhydride

isoborneol

di-(-)-bornyl 1,1,3,3-tetramethyl-1,3-acetonedicarboxylate

endo-borneol

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