Ethyl 3-(2,3-dihydro-1,4-benzodioxin-6-yl)-3-oxopropanoate

Base Information

Chemical Name:Ethyl 3-(2,3-dihydro-1,4-benzodioxin-6-yl)-3-oxopropanoate
CAS No.:74053-94-4
Molecular Formula:C₁₃H₁₄O₅
Molecular Weight:250.251
Hs Code.:
DSSTox Substance ID:DTXSID601220348

Synonyms:74053-94-4;ethyl 3-(2,3-dihydro-1,4-benzodioxin-6-yl)-3-oxopropanoate;ETHYL [3,4-(ETHYLENEDIOXY)BENZOYL]ACETATE;ethyl 3-(2,3-dihydrobenzo[b][1,4]dioxin-6-yl)-3-oxopropanoate;SCHEMBL13516438;VDROKCHVNRTMFA-UHFFFAOYSA-N;DTXSID601220348;3-(2,3-dihydro-benzo[1,4]dioxin-6-yl)-3-oxo-propionic acid ethyl ester

Suppliers and Price of Ethyl 3-(2,3-dihydro-1,4-benzodioxin-6-yl)-3-oxopropanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Labseeker
ETHYL[3,4-(ETHYLENEDIOXY)BENZOYL]ACETATE 95
25g
$ 3245.00

American Custom Chemicals Corporation
ETHYL [3,4-(ETHYLENEDIOXY) BENZOYL] ACETATE 95.00%
5MG
$ 497.57

Total 3 raw suppliers

Chemical Property of Ethyl 3-(2,3-dihydro-1,4-benzodioxin-6-yl)-3-oxopropanoate

Chemical Property:

Boiling Point:377.1±42.0 °C(Predicted)
PKA:10.76±0.20(Predicted)
Density:1.233±0.06 g/cm3(Predicted)
XLogP3:0.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:5
Exact Mass:250.08412354
Heavy Atom Count:18
Complexity:315

Purity/Quality:

99% ^*data from raw suppliers

ETHYL[3,4-(ETHYLENEDIOXY)BENZOYL]ACETATE 95 ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCOC(=O)CC(=O)C1=CC2=C(C=C1)OCCO2

Technology Process of Ethyl 3-(2,3-dihydro-1,4-benzodioxin-6-yl)-3-oxopropanoate

There total 7 articles about Ethyl 3-(2,3-dihydro-1,4-benzodioxin-6-yl)-3-oxopropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6761-70-2
2,3-dihydro-1,4-benzodioxine-6-carbonyl chloride

: 6148-64-7
ethyl potassium malonate

: 74053-94-4
ethyl 3-(2,3-dihydrobenzo[b][1,4]dioxin-6-yl)-3-oxopropanoate

Guidance literature:: ethyl potassium malonate; With N-ethyl-N,N-diisopropylamine; magnesium chloride; In dichloromethane; at 28 ℃; for 4h;

2,3-dihydro-1,4-benzodioxine-6-carbonyl chloride; In dichloromethane; at 0 ℃; for 0.166667h; under 760.051 Torr;

Reference yield:

: 1282295-32-2
C₁₂H₁₀N₂O₃

: 6148-64-7
ethyl potassium malonate

: 74053-94-4
ethyl 3-(2,3-dihydrobenzo[b][1,4]dioxin-6-yl)-3-oxopropanoate

Guidance literature:: ethyl potassium malonate; With dmap; triethylamine; magnesium chloride; In dichloromethane; at 28 ℃; for 5h;

C₁₂H₁₀N₂O₃; In dichloromethane; at 0 ℃; for 0.166667h; under 760.051 Torr;