Technology Process of C13H14N4O
There total 6 articles about C13H14N4O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine; methanol;
In
ISOPROPYLAMIDE; acetonitrile;
at 65 ℃;
for 2.5h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: potassium tert-butylate / toluene / 1.17 h / 20 °C / Cooling with ice
1.2: pH ~ 1
2.1: hydrazine hydrate / methanol / 2.5 h / Reflux
3.1: methanol / 1 h / 20 °C
4.1: hydroxylamine hydrochloride; sodium methylate / methanol / 17.5 h / 20 - 65 °C
5.1: pyridine / acetonitrile; ISOPROPYLAMIDE / 0.72 h / 20 °C
6.1: pyridine; methanol / acetonitrile; ISOPROPYLAMIDE / 2.5 h / 65 °C
With
pyridine; methanol; hydroxylamine hydrochloride; potassium tert-butylate; sodium methylate; hydrazine hydrate;
In
methanol; ISOPROPYLAMIDE; toluene; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: methanol / 1 h / 20 °C
2: hydroxylamine hydrochloride; sodium methylate / methanol / 17.5 h / 20 - 65 °C
3: pyridine / acetonitrile; ISOPROPYLAMIDE / 0.72 h / 20 °C
4: pyridine; methanol / acetonitrile; ISOPROPYLAMIDE / 2.5 h / 65 °C
With
pyridine; methanol; hydroxylamine hydrochloride; sodium methylate;
In
methanol; ISOPROPYLAMIDE; acetonitrile;