C₁₄H₂₁Cl

Base Information

Chemical Name:C₁₄H₂₁Cl
CAS No.:1010685-60-5
Molecular Formula:C₁₄H₂₁Cl
Molecular Weight:224.774
Hs Code.:

Synonyms:C₁₄H₂₁Cl

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Chemical Property of C₁₄H₂₁Cl

Chemical Property:

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Technology Process of C₁₄H₂₁Cl

There total 3 articles about C₁₄H₂₁Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 42371-64-2
9-hexyl-9-borabicyclo[3.3.1]nonane

: 222016-65-1
1-Chloro-1-iodo-2-phenylethane

: 1010685-60-5
C₁₄H₂₁Cl

Guidance literature:: With (1,2-dimethoxyethane)dichloronickel(II); potassium tert-butylate; (1R,2R)-(+)-N,N'-dimethyl-1,2-diphenyl-ethylenediamine; In 2-methyl-propan-1-ol; di-isopropyl ether; at 20 ℃; for 24h;
DOI:10.1039/c5sc04378f

Reference yield:

: 111-66-0,25068-25-1
oct-1-ene

: 960-16-7
tributylphenylstannane

: C₁₄H₂₁Cl

: 1010685-60-5
C₁₄H₂₁Cl

: 21948-46-9,72778-28-0
1,2-dichlorooctane

: 1-Phenyl-1-chlorooctan

Guidance literature:: With (Dichloroiodo)benzene; bis(benzonitrile)palladium(II) dichloride; In dichloromethane; at -78 - 20 ℃; for 13h; Title compound not separated from byproducts.;
DOI:10.1021/ja0782798

Reference yield:

: 7474-06-8,41998-38-3,94347-44-1,20334-70-7
2-chloro-3-phenylpropionic acid

: 1010685-60-5
C₁₄H₂₁Cl

Guidance literature:: Multi-step reaction with 2 steps

1: 1,3-Diiodo-5,5-dimethyl-2,4-imidazolidinedione / Irradiation

2: potassium tert-butylate; (1R,2R)-(+)-N,N'-dimethyl-1,2-diphenyl-ethylenediamine; (1,2-dimethoxyethane)dichloronickel(II) / di-isopropyl ether; 2-methyl-propan-1-ol / 24 h / 20 °C

With 1,3-Diiodo-5,5-dimethyl-2,4-imidazolidinedione; (1,2-dimethoxyethane)dichloronickel(II); potassium tert-butylate; (1R,2R)-(+)-N,N'-dimethyl-1,2-diphenyl-ethylenediamine; In 2-methyl-propan-1-ol; di-isopropyl ether;
DOI:10.1039/c5sc04378f