5-(5-(4-(N,N-bis(4-hexyloxyphenyl)amino)phenyl)thiophene-2-yl)thiophene

Base Information

Chemical Name:5-(5-(4-(N,N-bis(4-hexyloxyphenyl)amino)phenyl)thiophene-2-yl)thiophene
CAS No.:1256844-72-0
Molecular Formula:C₃₈H₄₃NO₂S₂
Molecular Weight:609.897
Hs Code.:

Synonyms:5-(5-(4-(N,N-bis(4-hexyloxyphenyl)amino)phenyl)thiophene-2-yl)thiophene

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Chemical Property of 5-(5-(4-(N,N-bis(4-hexyloxyphenyl)amino)phenyl)thiophene-2-yl)thiophene

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Technology Process of 5-(5-(4-(N,N-bis(4-hexyloxyphenyl)amino)phenyl)thiophene-2-yl)thiophene

There total 7 articles about 5-(5-(4-(N,N-bis(4-hexyloxyphenyl)amino)phenyl)thiophene-2-yl)thiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1092363-75-1
N,N-bis(4-hexyloxyphenyl)-4-bromophenylamine

: 479719-88-5
2-([2,2'-bithiophen]-5-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1256844-72-0
5-(5-(4-(N,N-bis(4-hexyloxyphenyl)amino)phenyl)thiophene-2-yl)thiophene

Guidance literature:: N,N-bis(4-hexyloxyphenyl)-4-bromophenylamine; 2-([2,2'-bithiophen]-5-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane; With potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri tert-butylphosphoniumtetrafluoroborate; In tetrahydrofuran; water; at 20 ℃; Inert atmosphere;

With potassium phosphate; In water; at 20 ℃;
DOI:10.1002/adfm.201102519

Reference yield: 60.0%

: 1092363-75-1
N,N-bis(4-hexyloxyphenyl)-4-bromophenylamine

: 133144-35-1
[2,2′-bithiophen]-5-yltrimethylstannane

: 1256844-72-0
5-(5-(4-(N,N-bis(4-hexyloxyphenyl)amino)phenyl)thiophene-2-yl)thiophene

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; for 24h; Reflux; Inert atmosphere;
DOI:10.1016/j.tet.2012.12.071

Reference yield:

: 1092363-75-1
N,N-bis(4-hexyloxyphenyl)-4-bromophenylamine

: 492-97-7
2,2'-Bithiophene

: 1256844-72-0
5-(5-(4-(N,N-bis(4-hexyloxyphenyl)amino)phenyl)thiophene-2-yl)thiophene

Guidance literature:: 2,2'-Bithiophene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 2h;

With trimethyltin(IV)chloride; In tetrahydrofuran; hexane; at -78 - 20 ℃;

N,N-bis(4-hexyloxyphenyl)-4-bromophenylamine; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; for 48h; Reflux; Inert atmosphere;
DOI:10.1021/ol102127x