(5S,7S)-5-Benzyloxycarbonylamino-7-[4-methoxy-3-(3-methoxy-propoxy)-benzyl]-8-methyl-4-oxo-nonanoic acid methyl ester

Base Information

Chemical Name:(5S,7S)-5-Benzyloxycarbonylamino-7-[4-methoxy-3-(3-methoxy-propoxy)-benzyl]-8-methyl-4-oxo-nonanoic acid methyl ester
CAS No.:900811-43-0
Molecular Formula:C₃₁H₄₃NO₈
Molecular Weight:557.684
Hs Code.:

Synonyms:(5S,7S)-5-Benzyloxycarbonylamino-7-[4-methoxy-3-(3-methoxy-propoxy)-benzyl]-8-methyl-4-oxo-nonanoic acid methyl ester

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Chemical Property of (5S,7S)-5-Benzyloxycarbonylamino-7-[4-methoxy-3-(3-methoxy-propoxy)-benzyl]-8-methyl-4-oxo-nonanoic acid methyl ester

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Technology Process of (5S,7S)-5-Benzyloxycarbonylamino-7-[4-methoxy-3-(3-methoxy-propoxy)-benzyl]-8-methyl-4-oxo-nonanoic acid methyl ester

There total 6 articles about (5S,7S)-5-Benzyloxycarbonylamino-7-[4-methoxy-3-(3-methoxy-propoxy)-benzyl]-8-methyl-4-oxo-nonanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 900811-42-9
pyridin-4-yl (2S,4S)-2-[[(phenylmethoxy)carbonyl]amino]-4-methoxy-3-(3-methoxypropoxy)-γ-(1-methylethyl)benzenepentanethioate

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 900811-43-0
(5S,7S)-5-Benzyloxycarbonylamino-7-[4-methoxy-3-(3-methoxy-propoxy)-benzyl]-8-methyl-4-oxo-nonanoic acid methyl ester

Guidance literature:: With samarium diiodide; tert-butyl alcohol; In tetrahydrofuran; at -78 ℃; for 144h;
DOI:10.1021/jo060296c

Reference yield:

: 900811-40-7
methyl (2S,4S)-2-[[(phenylmethoxy)carbonyl]amino]-4-methoxy-3-(3-methoxypropoxy)-γ-(1-methylethyl)benzenepentanoate

: 900811-43-0
(5S,7S)-5-Benzyloxycarbonylamino-7-[4-methoxy-3-(3-methoxy-propoxy)-benzyl]-8-methyl-4-oxo-nonanoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: aq. NaOH / tetrahydrofuran; methanol / 3.5 h / 20 °C

2: 94 percent / EDCI / CH₂Cl₂ / 3.5 h / 0 °C

3: 67 percent / t-BuOH; SmI₂ / tetrahydrofuran / 144 h / -78 °C

With sodium hydroxide; samarium diiodide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; tert-butyl alcohol; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jo060296c

Reference yield:

: 900811-41-8
(2S,4S)-2-[[(phenylmethoxy)carbonyl]amino]-4-methoxy-3-(3-methoxypropoxy)-γ-(1-methylethyl)benzenepentanoic acid

: 900811-43-0
(5S,7S)-5-Benzyloxycarbonylamino-7-[4-methoxy-3-(3-methoxy-propoxy)-benzyl]-8-methyl-4-oxo-nonanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / EDCI / CH₂Cl₂ / 3.5 h / 0 °C

2: 67 percent / t-BuOH; SmI₂ / tetrahydrofuran / 144 h / -78 °C

With samarium diiodide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; tert-butyl alcohol; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo060296c