1,2,3,4-tetra-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-α/β-D-glucopyranose

Base Information

• Chemical Name: 1,2,3,4-tetra-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-α/β-D-glucopyranose
• CAS No.: 544686-94-4
• Molecular Formula: C₆₈H₅₄O₁₉
• Molecular Weight: 1175.17

Synonyms:1,2,3,4-tetra-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-α/β-D-glucopyranose

Chemical Property of 1,2,3,4-tetra-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-α/β-D-glucopyranose

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of 1,2,3,4-tetra-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-α/β-D-glucopyranose

There total 7 articles about 1,2,3,4-tetra-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-α/β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

1,2,3,4-tetra-O-benzoyl-D-glucopyranoside (590367-95-6) + 2,3,4,6-tetra-O-benzoyl-D-glucopyranosyl 1-(N-phenyl)-2,2,2-trifluoroacetimidate (339276-12-9) → 1,2,3,4-tetra-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-α/β-D-glucopyranose (544686-94-4)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; In dichloromethane; at 20 ℃; for 8h;

DOI:10.1021/jo034223u

Reference yield: 98.0%

gentibiose (536-11-8,645-03-4,902-54-5,3031-35-4,4604-26-6,5340-95-4,5995-99-3,5996-00-9,13299-20-2,13299-21-3,15548-40-0,16750-26-8,16967-97-8,23339-29-9,24822-33-1,33428-65-8,34674-94-7,35867-21-1,37169-69-0,37169-72-5,38533-27-6,50271-70-0,65207-30-9,82729-73-5,95463-59-5,100427-99-4,100430-37-3,100483-14-5,102572-70-3,110658-40-7,123809-47-2,140461-60-5,143615-15-0) + benzoyl chloride (98-88-4) → 1,2,3,4-tetra-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-α/β-D-glucopyranose (544686-94-4)

Guidance literature:

With pyridine; at 40 ℃;

DOI:10.1016/j.bmc.2006.05.055

Reference yield: 94.0%

1,2,3,4-tetra-O-benzoyl-D-glucopyranoside (590367-95-6) + 2,3,4,6-tetra-O-benzoyl-D-glucopyranosyl trichloroacetimidate (149707-75-5) → 1,2,3,4-tetra-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-α/β-D-glucopyranose (544686-94-4)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃;

DOI:10.1016/j.carres.2009.04.024

upstream raw materials:

1,2,3,4-tetra-O-benzoyl-D-glucopyranoside

2,3,4,6-tetra-O-benzoyl-D-glucopyranosyl 1-(N-phenyl)-2,2,2-trifluoroacetimidate

gentibiose

benzoyl chloride

Downstream raw materials:

C₆₁H₄₉BrO₁₇

2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-D-glucopyranosyl (N-phenyl)trifluoroacetimidate

1,2-O-isopropylidene-3-O-[6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-2,3,4-tri-O-benzoyl-β-D-glucopyranosyl]-sn-glycerol

1,2-O-isopropylidene-3-O-[6-O-(6-O-tert-butyldiphenylsilyl-β-D-glucopyranosyl)-β-D-glucopyranosyl]-sn-glycerol

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