C₈₈H₁₂₈N₈O₂₄S₈Zn

Base Information

• Chemical Name: C₈₈H₁₂₈N₈O₂₄S₈Zn
• CAS No.: 956272-52-9
• Molecular Formula: C₈₈H₁₂₈N₈O₂₄S₈Zn
• Molecular Weight: 2003.94
• Mol file: 956272-52-9.mol

Synonyms:C₈₈H₁₂₈N₈O₂₄S₈Zn

Chemical Property of C₈₈H₁₂₈N₈O₂₄S₈Zn

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₈₈H₁₂₈N₈O₂₄S₈Zn

There total 3 articles about C₈₈H₁₂₈N₈O₂₄S₈Zn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

4,5-bis(4′,7′,10′-trioxaundecylsulfanyl)phthalonitrile (314263-26-8) + C59H55N6O7Pol → C88H128N8O24S8Zn (956272-52-9) + C125H151N12O25PolS6Zn

Guidance literature:

With zinc diacetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In butan-1-ol; at 25 - 150 ℃; for 0.75h; Microwave irradiation; solid phase reaction;

DOI:10.1021/jo901424v

Reference yield: 16.0%

4,5-bis(4′,7′,10′-trioxaundecylsulfanyl)phthalonitrile (314263-26-8) + 4-(mercapto benzoic acid)phthalonitrile + zinc diacetate (557-34-6) → C88H128N8O24S8Zn (956272-52-9) + 2-(4-mercapto benzoic acid) 9,10,16,17,23,24-(1-mercapto-4,7,10-trioxaundecane) Zn(II) phthalocyanine

Guidance literature:

4,5-bis(4′,7′,10′-trioxaundecylsulfanyl)phthalonitrile; 4-(mercapto benzoic acid)phthalonitrile; With 2-(N,N-dimethylamino)ethanol; for 0.333333h; Inert atmosphere;

zinc diacetate; for 3h; Reflux;

DOI:10.1142/S1088424614500709

Reference yield: 16.0%

4-(mercapto benzoic acid)phthalonitrile + 4,5-bis(4,7,10-trioxaundecane-1-sulfenyl)phthalonitrile + zinc diacetate (557-34-6) → C88H128N8O24S8Zn (956272-52-9) + 2-(4-mercapto benzoic acid) 9,10,16,17,23,24-(1-mercapto-4,7,10-trioxaundecane) Zn(II) phthalocyanine

Guidance literature:

4-(mercapto benzoic acid)phthalonitrile; 4,5-bis(4,7,10-trioxaundecane-1-sulfenyl)phthalonitrile; for 0.333333h; Inert atmosphere;

zinc diacetate; for 3h; Reflux; Inert atmosphere;

DOI:10.1142/S1088424614500709

upstream raw materials:

4,5-bis(4′,7′,10′-trioxaundecylsulfanyl)phthalonitrile

zinc diacetate