(R)-benzyl 1-(1-amino-2-methylallyl)cyclopropylcarbamate hydrochloride

Base Information

Chemical Name:(R)-benzyl 1-(1-amino-2-methylallyl)cyclopropylcarbamate hydrochloride
CAS No.:1439908-67-4
Molecular Formula:C₁₅H₂₀N₂O₂*ClH
Molecular Weight:296.797
Hs Code.:

Synonyms:(R)-benzyl 1-(1-amino-2-methylallyl)cyclopropylcarbamate hydrochloride

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Chemical Property of (R)-benzyl 1-(1-amino-2-methylallyl)cyclopropylcarbamate hydrochloride

Chemical Property:

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Technology Process of (R)-benzyl 1-(1-amino-2-methylallyl)cyclopropylcarbamate hydrochloride

There total 5 articles about (R)-benzyl 1-(1-amino-2-methylallyl)cyclopropylcarbamate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: benzyl 1-((R)-1-((R)-1,1-dimethylethylsulfinamido)-2-methylallyl)cyclopropylcarbamate

: 1439908-67-4
(R)-benzyl 1-(1-amino-2-methylallyl)cyclopropylcarbamate hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; methanol; for 0.5h;

Reference yield:

: 84677-06-5
(benzyloxycarbonylamino)cyclopropanecarboxylic acid

: 1439908-67-4
(R)-benzyl 1-(1-amino-2-methylallyl)cyclopropylcarbamate hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide / 2 h / 20 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 °C

3: titanium(IV) tetraethanolate / tetrahydrofuran / 4 h

4: tetrahydrofuran; dichloromethane / 1 h / 0 °C / Inert atmosphere

5: hydrogenchloride / 1,4-dioxane; methanol / 0.5 h

With hydrogenchloride; titanium(IV) tetraethanolate; lithium aluminium tetrahydride; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 851726-81-3
benzyl {1-[methoxy(methyl)carbamoyl]cyclopropyl}carbamate

: 1439908-67-4
(R)-benzyl 1-(1-amino-2-methylallyl)cyclopropylcarbamate hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 °C

2: titanium(IV) tetraethanolate / tetrahydrofuran / 4 h

3: tetrahydrofuran; dichloromethane / 1 h / 0 °C / Inert atmosphere

4: hydrogenchloride / 1,4-dioxane; methanol / 0.5 h

With hydrogenchloride; titanium(IV) tetraethanolate; lithium aluminium tetrahydride; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane;