(7E)-7-{[4-(methylsulfanyl)phenyl]methylidene}-5,6,7,8-tetrahydroindolizin-8-one

Base Information

• Chemical Name: (7E)-7-{[4-(methylsulfanyl)phenyl]methylidene}-5,6,7,8-tetrahydroindolizin-8-one
• CAS No.: 1590380-45-2
• Molecular Formula: C₁₆H₁₅NOS
• Molecular Weight: 269.367

Synonyms:(7E)-7-{[4-(methylsulfanyl)phenyl]methylidene}-5,6,7,8-tetrahydroindolizin-8-one

Chemical Property of (7E)-7-{[4-(methylsulfanyl)phenyl]methylidene}-5,6,7,8-tetrahydroindolizin-8-one

Chemical Property:

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Technology Process of (7E)-7-{[4-(methylsulfanyl)phenyl]methylidene}-5,6,7,8-tetrahydroindolizin-8-one

There total 1 articles about (7E)-7-{[4-(methylsulfanyl)phenyl]methylidene}-5,6,7,8-tetrahydroindolizin-8-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

1-Azabicyclo[4.3.0]nona-6,8-diene-5-one (54906-44-4) + 4-(Methylthio)benzaldehyde (3446-89-7) → (7E)-7-{[4-(methylsulfanyl)phenyl]methylidene}-5,6,7,8-tetrahydroindolizin-8-one (1590380-45-2)

Guidance literature:

With sodium hydroxide; In ethanol; water; at 45 ℃; for 2h;

DOI:10.3184/174751913X13814138618396

Reference yield: 83.0%

11H-Indeno[1,2-b]quinoxaline-11-one (6954-91-2) + (7E)-7-{[4-(methylsulfanyl)phenyl]methylidene}-5,6,7,8-tetrahydroindolizin-8-one (1590380-45-2) + L-proline (147-85-3,25191-13-3,37159-97-0,4305-67-3,4607-28-7) → 1′-[4-(methylsulfanyl)phenyl]-5′,5″,6′,6″,7′,7a′-hexahydro-1′H,8″H-dispiro[indeno[1,2-b]quinoxaline-11,3′-pyrrolizine-2′,7″-indolizin]-8″-one

Guidance literature:

In methanol; for 1h; Reflux;

DOI:10.1134/S1070428021100237

Reference yield: 73.0%

(7E)-7-{[4-(methylsulfanyl)phenyl]methylidene}-5,6,7,8-tetrahydroindolizin-8-one (1590380-45-2) + thiourea (17356-08-0) → 4-[4- (methylthio)phenyl]-3,4,5,6-tetrahydropyrimido[5,4-g]indolizine-2(1H)-thione

Guidance literature:

With potassium hydroxide; In ethanol; at 80 ℃; for 2h;

DOI:10.3184/174751918X15426288948686

upstream raw materials:

1-Azabicyclo[4.3.0]nona-6,8-diene-5-one

4-(Methylthio)benzaldehyde

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