C₃₀H₂₈N₂O₅

Base Information

Chemical Name:C₃₀H₂₈N₂O₅
CAS No.:1620069-68-2
Molecular Formula:C₃₀H₂₈N₂O₅
Molecular Weight:496.563
Hs Code.:

C<sub>30</sub>H<sub>28</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:C₃₀H₂₈N₂O₅

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Chemical Property of C₃₀H₂₈N₂O₅

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Technology Process of C₃₀H₂₈N₂O₅

There total 8 articles about C₃₀H₂₈N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1620074-35-2
C₃₁H₃₀N₂O₅

: 1620069-68-2
C₃₀H₂₈N₂O₅

Guidance literature:: C₃₁H₃₀N₂O₅; With lithium hydroxide; In methanol; water; at 20 ℃;

With hydrogenchloride; In methanol; water; pH=4.0;

Reference yield:

: 638220-35-6
1-(4-bromophenyl)-cyclopropanecarboxylic acid methyl ester

: 1620069-68-2
C₃₀H₂₈N₂O₅

Guidance literature:: Multi-step reaction with 8 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / -4 °C

2.1: triethylamine / dichloromethane / 3 h / -78 - 0 °C

3.1: triethylamine / N,N-dimethyl-formamide / 3 h / 70 °C

4.1: sodium hydroxide / methanol; water / 16 h / 60 °C

4.2: pH 3

5.1: hydrogenchloride / 18 h / Reflux

6.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / Inert atmosphere; Reflux

7.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,2-dimethoxyethane / 4 h / Inert atmosphere; Reflux

8.1: lithium hydroxide / methanol; water / 20 °C

8.2: pH 4.0

With hydrogenchloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; lithium aluminium tetrahydride; potassium acetate; sodium carbonate; triethylamine; sodium hydroxide; lithium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; 1,2-dimethoxyethane; dichloromethane; water; N,N-dimethyl-formamide; 7.1: |Suzuki Coupling;

Reference yield:

: C₁₁H₁₃BrO₃S

: 1620069-68-2
C₃₀H₂₈N₂O₅

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine / N,N-dimethyl-formamide / 3 h / 70 °C

2.1: sodium hydroxide / methanol; water / 16 h / 60 °C

2.2: pH 3

3.1: hydrogenchloride / 18 h / Reflux

4.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / Inert atmosphere; Reflux

5.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,2-dimethoxyethane / 4 h / Inert atmosphere; Reflux

6.1: lithium hydroxide / methanol; water / 20 °C

6.2: pH 4.0

With hydrogenchloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; sodium carbonate; triethylamine; sodium hydroxide; lithium hydroxide; In 1,4-dioxane; methanol; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; 5.1: |Suzuki Coupling;