(Z)-1-[3',5'-dimethoxy-4'-[(tert-butyldimethylsilyl)oxy]phenyl]-2-[2,3-di-[(isopropyl)oxy]-4-methoxyphenyl]ethene

Base Information

Chemical Name:(Z)-1-[3',5'-dimethoxy-4'-[(tert-butyldimethylsilyl)oxy]phenyl]-2-[2,3-di-[(isopropyl)oxy]-4-methoxyphenyl]ethene
CAS No.:1116459-89-2
Molecular Formula:C₂₉H₄₄O₆Si
Molecular Weight:516.75
Hs Code.:

Synonyms:(Z)-1-[3',5'-dimethoxy-4'-[(tert-butyldimethylsilyl)oxy]phenyl]-2-[2,3-di-[(isopropyl)oxy]-4-methoxyphenyl]ethene

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Chemical Property of (Z)-1-[3',5'-dimethoxy-4'-[(tert-butyldimethylsilyl)oxy]phenyl]-2-[2,3-di-[(isopropyl)oxy]-4-methoxyphenyl]ethene

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Technology Process of (Z)-1-[3',5'-dimethoxy-4'-[(tert-butyldimethylsilyl)oxy]phenyl]-2-[2,3-di-[(isopropyl)oxy]-4-methoxyphenyl]ethene

There total 1 articles about (Z)-1-[3',5'-dimethoxy-4'-[(tert-butyldimethylsilyl)oxy]phenyl]-2-[2,3-di-[(isopropyl)oxy]-4-methoxyphenyl]ethene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 1116460-14-0
2,3-di[(isopropyl)oxy]-4-methoxybenzyltriphenylphosphonium bromide

: 106852-80-6
4-(t-butyldimethylsilyloxy)-3,5-dimethoxybenzaldehyde

: 1116459-89-2
(Z)-1-[3',5'-dimethoxy-4'-[(tert-butyldimethylsilyl)oxy]phenyl]-2-[2,3-di-[(isopropyl)oxy]-4-methoxyphenyl]ethene

: 1116459-91-6
(E)-1-[3',5'-dimethoxy-4'-[(tert-butyldimethylsilyl)oxy]phenyl]-2-[2'',3''-di[(isopropyl)oxy]-4''-methoxyphenyl]ethene

Guidance literature:: 2,3-di[(isopropyl)oxy]-4-methoxybenzyltriphenylphosphonium bromide; With n-butyllithium; In tetrahydrofuran; hexane; at -10 ℃;

4-(t-butyldimethylsilyloxy)-3,5-dimethoxybenzaldehyde; In tetrahydrofuran; hexane; at -78 - 0 ℃;
DOI:10.1021/np800661r

Reference yield: 89.0%

: 1116459-89-2
(Z)-1-[3',5'-dimethoxy-4'-[(tert-butyldimethylsilyl)oxy]phenyl]-2-[2,3-di-[(isopropyl)oxy]-4-methoxyphenyl]ethene

: 74-88-4
methyl iodide

: 1400573-38-7
(Z)-1-[3',4',5'-trimethoxyphenyl]-2-[2'',3''-di[(isopropyl)oxy]-4''-methoxyphenyl]ethene

Guidance literature:: With tetrabutyl ammonium fluoride; In acetonitrile; at 0 ℃;
DOI:10.1021/np800661r

Reference yield: 75.0%

: 16170-82-4
[14C]methyl iodide

: 1116459-89-2
(Z)-1-[3',5'-dimethoxy-4'-[(tert-butyldimethylsilyl)oxy]phenyl]-2-[2,3-di-[(isopropyl)oxy]-4-methoxyphenyl]ethene

: 1116460-16-2
(Z)-1-[3',[4'-14C],5'-trimethoxyphenyl]-2-[2'',3''-di-[(isopropyl)oxy]-4''-methoxyphenyl]ethene

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; acetonitrile; at 0 ℃; for 0.5h; Molecular sieve;
DOI:10.1002/JLCR.1676