benzyl 2-(tert-butoxycarbonylamino)-3-(3-formyl-4-hydroxyphenyl)propanoate

Base Information

Chemical Name:benzyl 2-(tert-butoxycarbonylamino)-3-(3-formyl-4-hydroxyphenyl)propanoate
CAS No.:1215819-56-9
Molecular Formula:C₂₂H₂₅NO₆
Molecular Weight:399.444
Hs Code.:

Synonyms:benzyl 2-(tert-butoxycarbonylamino)-3-(3-formyl-4-hydroxyphenyl)propanoate

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Chemical Property of benzyl 2-(tert-butoxycarbonylamino)-3-(3-formyl-4-hydroxyphenyl)propanoate

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Technology Process of benzyl 2-(tert-butoxycarbonylamino)-3-(3-formyl-4-hydroxyphenyl)propanoate

There total 1 articles about benzyl 2-(tert-butoxycarbonylamino)-3-(3-formyl-4-hydroxyphenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 186689-03-2
2-(tert-butoxycarbonylamino)-3-(3-formyl-4-hydroxyphenyl)propanoic acid

: 100-51-6,185532-71-2
benzyl alcohol

: 1215819-56-9
benzyl 2-(tert-butoxycarbonylamino)-3-(3-formyl-4-hydroxyphenyl)propanoate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 - 20 ℃; for 3.5h;
DOI:10.1039/b919744c

Reference yield: 70.0%

: 1215819-56-9
benzyl 2-(tert-butoxycarbonylamino)-3-(3-formyl-4-hydroxyphenyl)propanoate

: 814-49-3
diethyl chlorophosphate

: 1215819-57-0
benzyl 2-(tert-butoxycarbonylamino)-3-(4-(diethoxyphosphoryloxy)-3-formylphenyl)propanoate

Guidance literature:: benzyl 2-(tert-butoxycarbonylamino)-3-(3-formyl-4-hydroxyphenyl)propanoate; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 ℃; for 0.25h; Inert atmosphere;

diethyl chlorophosphate; at 20 ℃; for 8.75h; Cooling with ice;
DOI:10.1039/b919744c