6-chloro-2-(3''-(1''-(p-toluenesulfonyl)pyrrolyl)ethyloxy)-3',4',5'-triacetyladenosine

Base Information

Chemical Name:6-chloro-2-(3''-(1''-(p-toluenesulfonyl)pyrrolyl)ethyloxy)-3',4',5'-triacetyladenosine
CAS No.:936252-89-0
Molecular Formula:C₂₉H₃₀ClN₅O₁₀S
Molecular Weight:676.104
Hs Code.:

Synonyms:6-chloro-2-(3''-(1''-(p-toluenesulfonyl)pyrrolyl)ethyloxy)-3',4',5'-triacetyladenosine

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Chemical Property of 6-chloro-2-(3''-(1''-(p-toluenesulfonyl)pyrrolyl)ethyloxy)-3',4',5'-triacetyladenosine

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Technology Process of 6-chloro-2-(3''-(1''-(p-toluenesulfonyl)pyrrolyl)ethyloxy)-3',4',5'-triacetyladenosine

There total 4 articles about 6-chloro-2-(3''-(1''-(p-toluenesulfonyl)pyrrolyl)ethyloxy)-3',4',5'-triacetyladenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 936252-72-1
3-(2-iodoethyl)-1-(p-toluenesulfonyl)pyrrole

: 161923-50-8
6-chloro-2-hydroxy-9-(2,3,5-tri-O-acetyl-β-D-ribofuranosyl) purine

: 936252-89-0
6-chloro-2-(3''-(1''-(p-toluenesulfonyl)pyrrolyl)ethyloxy)-3',4',5'-triacetyladenosine

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1021/jm061278q

Reference yield: 61.0%

: 936252-89-0
6-chloro-2-(3''-(1''-(p-toluenesulfonyl)pyrrolyl)ethyloxy)-3',4',5'-triacetyladenosine

Guidance literature:

Reference yield:

: 708259-63-6
3-(2-hydroxyethyl)-1-(p-toluenesulfonyl)pyrrole

: 936252-89-0
6-chloro-2-(3''-(1''-(p-toluenesulfonyl)pyrrolyl)ethyloxy)-3',4',5'-triacetyladenosine

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / lithium aluminum hydride / tetrahydrofuran / 2 h / 0 °C

2: 61 percent / Cs₂CO₃ / dimethylformamide / 20 °C

With lithium aluminium tetrahydride; caesium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm061278q