N-[(4-aminophenyl)(methyl)oxo-lambda6-sulfanylidene]-2,2,2-trifluoroacetamide

Base Information

Chemical Name:N-[(4-aminophenyl)(methyl)oxo-lambda6-sulfanylidene]-2,2,2-trifluoroacetamide
CAS No.:1223498-52-9
Molecular Formula:C₉H₉F₃N₂O₂S
Molecular Weight:266.244
Hs Code.:

Synonyms:N-[(4-aminophenyl)(methyl)oxo-lambda6-sulfanylidene]-2,2,2-trifluoroacetamide

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Chemical Property of N-[(4-aminophenyl)(methyl)oxo-lambda6-sulfanylidene]-2,2,2-trifluoroacetamide

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Technology Process of N-[(4-aminophenyl)(methyl)oxo-lambda6-sulfanylidene]-2,2,2-trifluoroacetamide

There total 3 articles about N-[(4-aminophenyl)(methyl)oxo-lambda6-sulfanylidene]-2,2,2-trifluoroacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 952022-17-2
N-(trifluoroacetyl)-S-methyl-S-(4-nitrophenyl)sulfoximine

: 1223498-52-9
N-[(4-aminophenyl)(methyl)oxo-lambda6-sulfanylidene]-2,2,2-trifluoroacetamide

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; di-isopropyl ether; at 24 ℃; for 0.75h; under 760.051 Torr;

Reference yield:

: 940-12-5
p-nitrophenyl methyl sulfoxide

: 1223498-52-9
N-[(4-aminophenyl)(methyl)oxo-lambda6-sulfanylidene]-2,2,2-trifluoroacetamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium azide; sulfuric acid / dichloromethane / 16 h / 0 - 45 °C

1.2: pH 11

2.1: dmap; triethylamine / dichloromethane / 2 h / cooling with ice

3.1: hydrogen / palladium 10% on activated carbon / di-isopropyl ether; ethanol; tetrahydrofuran / 0.75 h / 24 °C / 760.05 Torr

With dmap; sodium azide; sulfuric acid; hydrogen; triethylamine; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; dichloromethane; di-isopropyl ether;

Reference yield:

: 22133-01-3
S-methyl-S-(4-nitrophenyl)sulfoximine

: 1223498-52-9
N-[(4-aminophenyl)(methyl)oxo-lambda6-sulfanylidene]-2,2,2-trifluoroacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; triethylamine / dichloromethane / 2 h / cooling with ice

2: hydrogen / palladium 10% on activated carbon / di-isopropyl ether; ethanol; tetrahydrofuran / 0.75 h / 24 °C / 760.05 Torr

With dmap; hydrogen; triethylamine; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; dichloromethane; di-isopropyl ether;