tert-butyl(((3S,4R)-1-((4-methoxybenzyl)oxy)-4-methylhex-5-en-3-yl)oxy)dimethylsilane

Base Information

• Chemical Name: tert-butyl(((3S,4R)-1-((4-methoxybenzyl)oxy)-4-methylhex-5-en-3-yl)oxy)dimethylsilane
• CAS No.: 220249-56-9
• Molecular Formula: C₂₁H₃₆O₃Si
• Molecular Weight: 364.601

Synonyms:tert-butyl(((3S,4R)-1-((4-methoxybenzyl)oxy)-4-methylhex-5-en-3-yl)oxy)dimethylsilane

Chemical Property of tert-butyl(((3S,4R)-1-((4-methoxybenzyl)oxy)-4-methylhex-5-en-3-yl)oxy)dimethylsilane

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Technology Process of tert-butyl(((3S,4R)-1-((4-methoxybenzyl)oxy)-4-methylhex-5-en-3-yl)oxy)dimethylsilane

There total 10 articles about tert-butyl(((3S,4R)-1-((4-methoxybenzyl)oxy)-4-methylhex-5-en-3-yl)oxy)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

tert-butyldimethylsilyl chloride (18162-48-6) + (3S,4R)-1-(4-methoxybenzyloxy)-4-(trifluoromethyl)hex-5-en-3-ol (220249-55-8) → tert-butyl(((3S,4R)-1-((4-methoxybenzyl)oxy)-4-methylhex-5-en-3-yl)oxy)dimethylsilane (220249-56-9)

Guidance literature:

With 1H-imidazole; dmap; In N,N-dimethyl-formamide; at 60 ℃;

DOI:10.1016/S0960-894X(02)01023-5

Reference yield: 92.0%

t-butyldimethylsiyl triflate (69739-34-0) + (3S,4R)-1-(4-methoxybenzyloxy)-4-(trifluoromethyl)hex-5-en-3-ol (220249-55-8) → tert-butyl(((3S,4R)-1-((4-methoxybenzyl)oxy)-4-methylhex-5-en-3-yl)oxy)dimethylsilane (220249-56-9)

Guidance literature:

With 2,6-dimethylpyridine; In dichloromethane; at -78 ℃; for 0.166667h;

DOI:10.1021/jo000767+

Reference yield: 92.0%

t-butyldimethylsiyl triflate (69739-34-0) + 1-(4-methoxybenzyloxy)-4-methylhex-5-en-3-ol (849619-01-8) → tert-butyl(((3S,4R)-1-((4-methoxybenzyl)oxy)-4-methylhex-5-en-3-yl)oxy)dimethylsilane (220249-56-9)

Guidance literature:

With 2,6-dimethylpyridine; In tetrahydrofuran; at -78 ℃; for 0.166667h;

DOI:10.1016/S0960-894X(98)00557-5

upstream raw materials:

t-butyldimethylsiyl triflate

1-(4-methoxybenzyloxy)-4-methylhex-5-en-3-ol

(3S,4R)-1-(4-methoxybenzyloxy)-4-(trifluoromethyl)hex-5-en-3-ol

tert-butyldimethylsilyl chloride

Downstream raw materials:

4-methoxy-benzaldehyde

(3S,4R)-3-(tert-butyldimethylsilyloxy)-4-methylhex-5-en-1-ol

tert-butyl(((3S,4R)-1-((4-methoxybenzyl)oxy)-4-methyl-8-(trimethylsilyl)oct-7-yn-3-yl)oxy)dimethylsilane

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