C₂₅H₂₆N₆O₃S

Base Information

Chemical Name:C₂₅H₂₆N₆O₃S
CAS No.:1420997-73-4
Molecular Formula:C₂₅H₂₆N₆O₃S
Molecular Weight:490.586
Hs Code.:

C<sub>25</sub>H<sub>26</sub>N<sub>6</sub>O<sub>3</sub>S

Synonyms:C₂₅H₂₆N₆O₃S

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Chemical Property of C₂₅H₂₆N₆O₃S

Chemical Property:

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Technology Process of C₂₅H₂₆N₆O₃S

There total 11 articles about C₂₅H₂₆N₆O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 120-93-4
imidazolidone

: 1420998-39-5
N-{3-[5-(3-bromo-5-isopropoxy-phenyl)oxazol-2-ylamino]-4-methyl-phenyl}-N-thiazol-2-yl-acetamide

: 1420997-73-4
C₂₅H₂₆N₆O₃S

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; at 110 ℃; for 16h; Sealed tube;

Reference yield:

: 1420998-08-8
5-(3-bromo-5-isopropoxy-phenyl)oxazole

: 1420997-73-4
C₂₅H₂₆N₆O₃S

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: 16 h / -78 - 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 - 20 °C

2.2: 16 h / 0 - 20 °C

3.1: caesium carbonate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / 1,4-dioxane / 16 h / 110 °C / Sealed tube

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium hydride; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; lithium hexamethyldisilazane; In tetrahydrofuran; 1,4-dioxane; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 1435-51-4
1,3-dibromo-5-fluorobenzene

: 1420997-73-4
C₂₅H₂₆N₆O₃S

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 0 °C / Inert atmosphere

1.2: 16 h / 0 - 20 °C

2.1: n-butyllithium / diethyl ether / 0.5 h / -78 °C / Inert atmosphere

2.2: 1.5 h / -78 - -40 °C

3.1: potassium carbonate / methanol / 16 h / 20 °C

4.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

4.2: 16 h / -78 - 20 °C

5.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 - 20 °C

5.2: 16 h / 0 - 20 °C

6.1: caesium carbonate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / 1,4-dioxane / 16 h / 110 °C / Sealed tube

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; n-butyllithium; sodium hydride; potassium carbonate; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; lithium hexamethyldisilazane; In tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; N,N-dimethyl-formamide; mineral oil;