methyl N-phenyl-N-(2,2-diphenyl-1-t-butyldimethylsiloxy)-vinyl-carbamate

Base Information

Chemical Name:methyl N-phenyl-N-(2,2-diphenyl-1-t-butyldimethylsiloxy)-vinyl-carbamate
CAS No.:103707-72-8
Molecular Formula:C₂₈H₃₃NO₃Si
Molecular Weight:459.66
Hs Code.:

Synonyms:methyl N-phenyl-N-(2,2-diphenyl-1-t-butyldimethylsiloxy)-vinyl-carbamate

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Chemical Property of methyl N-phenyl-N-(2,2-diphenyl-1-t-butyldimethylsiloxy)-vinyl-carbamate

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Technology Process of methyl N-phenyl-N-(2,2-diphenyl-1-t-butyldimethylsiloxy)-vinyl-carbamate

There total 3 articles about methyl N-phenyl-N-(2,2-diphenyl-1-t-butyldimethylsiloxy)-vinyl-carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 525-06-4
diphenyl ketene

: 103707-73-9
methyl N-phenyl-N-t-butyldimethylsilylcarbamate

: 103707-72-8
methyl N-phenyl-N-(2,2-diphenyl-1-t-butyldimethylsiloxy)-vinyl-carbamate

Guidance literature:: In diethyl ether; at 0 ℃; for 20h;

Reference yield:

: 2603-10-3
N-phenyl methyl carbamate

: 103707-72-8
methyl N-phenyl-N-(2,2-diphenyl-1-t-butyldimethylsiloxy)-vinyl-carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / 1.) NaH / tetrahydrofuran / 1.) 0 deg C, 2.) -78 deg C to room temp., overnight

2: 85 percent / diethyl ether / 20 h / 0 °C

With sodium hydride; In tetrahydrofuran; diethyl ether;

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 103707-72-8
methyl N-phenyl-N-(2,2-diphenyl-1-t-butyldimethylsiloxy)-vinyl-carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / 1.) NaH / tetrahydrofuran / 1.) 0 deg C, 2.) -78 deg C to room temp., overnight

2: 85 percent / diethyl ether / 20 h / 0 °C

With sodium hydride; In tetrahydrofuran; diethyl ether;