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(2S,3R,5R)-3-Chlorocarbonyl-3-methyl-4,4,7-trioxo-4λ6-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylic acid benzhydryl ester

Base Information Edit
  • Chemical Name:(2S,3R,5R)-3-Chlorocarbonyl-3-methyl-4,4,7-trioxo-4λ6-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylic acid benzhydryl ester
  • CAS No.:1026477-53-1
  • Molecular Formula:C21H18ClNO6S
  • Molecular Weight:447.896
  • Hs Code.:
  • Mol file:1026477-53-1.mol
(2S,3R,5R)-3-Chlorocarbonyl-3-methyl-4,4,7-trioxo-4λ<sup>6</sup>-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylic acid benzhydryl ester

Synonyms:(2S,3R,5R)-3-Chlorocarbonyl-3-methyl-4,4,7-trioxo-4λ6-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylic acid benzhydryl ester

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Chemical Property of (2S,3R,5R)-3-Chlorocarbonyl-3-methyl-4,4,7-trioxo-4λ6-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylic acid benzhydryl ester Edit
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Technology Process of (2S,3R,5R)-3-Chlorocarbonyl-3-methyl-4,4,7-trioxo-4λ6-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylic acid benzhydryl ester

There total 8 articles about (2S,3R,5R)-3-Chlorocarbonyl-3-methyl-4,4,7-trioxo-4λ6-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylic acid benzhydryl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 10 steps
1: sulfuric acid; potassium bromide; sodium nitrite / ethanol / 3.5 h / 6 - 8 °C
2: peracetic acid; potassium iodide / dichloromethane; water / 1 h / 0 °C
3: acetic acid; zinc / acetonitrile / 1 h / 0 °C
4: toluene / 2 h / 114 °C
5: silver(I) acetate / dichloromethane / 4 h / 20 °C
6: potassium permanganate; acetic acid / water; acetone / 1 h / 20 °C
7: thiourea / ethanol / 1 h / 70 °C
8: Dess-Martin periodane / dichloromethane / 1 h / 20 °C
9: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / tetrahydrofuran; tert-butyl alcohol / 1 h / 20 °C
10: pyridine; oxalyl dichloride / dichloromethane / 1 h / 20 °C
With pyridine; peracetic acid; sodium chlorite; potassium permanganate; sodium dihydrogenphosphate; 2-methyl-but-2-ene; oxalyl dichloride; sulfuric acid; silver(I) acetate; Dess-Martin periodane; acetic acid; thiourea; potassium iodide; potassium bromide; zinc; sodium nitrite; In tetrahydrofuran; ethanol; dichloromethane; water; acetone; toluene; acetonitrile; tert-butyl alcohol;
DOI:10.1128/AAC.06099-11
Guidance literature:
Multi-step reaction with 3 steps
1: Dess-Martin periodane / dichloromethane / 1 h / 20 °C
2: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / tetrahydrofuran; tert-butyl alcohol / 1 h / 20 °C
3: pyridine; oxalyl dichloride / dichloromethane / 1 h / 20 °C
With pyridine; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; oxalyl dichloride; Dess-Martin periodane; In tetrahydrofuran; dichloromethane; tert-butyl alcohol;
DOI:10.1128/AAC.06099-11
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